HPLC Determination of Bulgarian Xinning Danshensu content of particles in the.docVIP

 PAGE \* MERGEFORMAT 7 HPLC Determination of Bulgarian Xinning Danshensu content of particles in the Author: Shen Gao Fang Lijun Jiang East China Sea [Abstract] Objective: To establish Baoxin Danshensu Granule method for the determination. Methods: HPLC determination of Danshensu content. Agilent C18 column for the column (250mm * 4.6mm, 5μ m), with water - methanol - acetic acid (88:12:0.05) as mobile phase, column temperature at room temperature, flow rate 1ml * min-1. Results: In the 2.0 ~ 10.0μ g Danshensu sample volume and the peak area has a good linear relationship. r = 0.9998 (n = 5), the average recovery was 97.5% (RSD = 0.61%). Conclusion: The method is high precision, reproducibility, and can be used to determine the content of Danshensu. [Keywords:] Bao-Xin Ning particles Danshensu high performance liquid chromatography Determination of the content of Danshensu in Baoxinning granules [Abstract] AIM: to estabolish the method to determine the Danshensu in Baoxinning granules.Methods: HPLC was used to determine the Danshensu.Agilent C18 (250mm * 4.6mm, 5μ m) as the chromatogram column.And water: methanol: acetic acid ( 90:10:0.05) as the mobile phase.1.0ml * min-1 folw rate, column temperature was room temperature.Results the calibration curves were linear in the ranger2.0 ~ 10μ m of Danshensu.The correlation coefficient was 0.9998 (n = 5), the average recovery rate was 97.5%, and the RSD was 0.61%. Conclusion: The method was simple, eccurate and can be used to determine the Danshensu in Baoxinning granules. [Key Words] Baoxinning granules; Danshensu; HPLC Bao Xin Bao Xin Ning Ning particles from the capsules through improved formulations come Baoxin Capsule is ‘the Ministry of Health standards for traditional Chinese medicine set prescription drug formulations’ (11th volumes) containing relevant species [1], from Salvia, 37, Angelica, Citrus aurantium composition, heart-protecting capsules with blood circulation, Qi analgesic effect, for