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- 2017-05-03 发布于浙江
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HPLC determination of clear pill capsules Bimin prime fat content of Mulan
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HPLC determination of clear pill capsules Bimin prime fat content of Mulan
Of: Li Jian, Zhou Jie, Zhi-Xiong Liu, Xudong Dong, Lai Keying
[Abstract] Objective To establish a clear pill capsules Bimin Mulan in determining the content of Lignans. Methods HPLC method: column was Diamonsil C18 (250 mm 4.6 mm, 5 m), mobile phase of acetonitrile tetrahydrofuran water (volume ratio 42: 2:56), flow rate 1.0 mL / min, column temperature was 35 , the detection wavelength was 278 nm. Results Mulan visfatin concentration in the 1.856 ~ 46.40 g / mL was linear within the range, the average recovery was 98.34%, RSD 1.53%. Conclusion The method is accurate, reproducible, and can be used to clear nasal sensitivity for the quality control pills.
[Keywords:] HPLC method, clear pill capsules Bimin Mulan visfatin, determination
Abstract: Objective To establish an HPLC method for the assay of magnolin in Biminqingwan capsules. Methods The analytical column was Diamonsil C18 (250 mm 4.6 mm, 0.5 m). The mobile phase consisted of CH3CN C4H8O H2O (42:2:56) . The flow rate was 1.0 mL / min and column temperature at 35 . The detection wavelength was 278 nm. Results The magnolin linearity range was 1.856-46.40 g / mL. The average recovery was 98.34%, and the RSD was 1.53%. Conclusion This method was simple, accurate and can be used for the quality control of Biminqingwan capsules.
Keywords:: HPLC; Biminqingwan capsules; magnolin; content determination
Clear pill capsules Bimin by the magnolia, patchouli, fruit, chrysanthemum etc., with increased body resistance to disease, and enhance anti-inflammatory, antibacterial, Quyu students new and rapid improvements in nasal tissue metabolism and the blood circulation, eliminate nasal fluid, the effect of concentration of tears, for the treatment of acute and chronic rhinitis, allergic rhinitis, forehead pain, hyposmia, and nasal speech, with symptoms such as [1]. relating to the preparation of quality c
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