Microwave Digestion - Atomic Fluorescence Spectrometry of Trace Arsenic in Polygonum.doc

 PAGE \* MERGEFORMAT 4 Microwave Digestion - Atomic Fluorescence Spectrometry of Trace Arsenic in Polygonum Author: Huang Fei, Qin Fan-xin, Hu Jiwei, Di, Yan Yuanzhi [Abstract] Objective To establish Polygonum trace arsenic in atomic fluorescence analysis. Method of microwave digestion and hydride generation atomic fluorescence spectrometry. Results The linear range of 0.002 ~ 0.120 mg / L, R = 0.999 8, the method recoveries were 86.8% ~ 109.6%, with an average recovery of 101.7% and precision RSD = 1.7%, detection limit of 0.040 mg / kg. Conclusion The method is simple, fast, safe, high sensitivity and good precision and accuracy, and can be widely used. [Keywords] microwave digestion; atomic fluorescence; Polygonum; Trace Arsenic AbstractObjectiveTo establish a method for determination of trace arsenic in Poligonum capitatum with atomic fluorescent spectrometry.MethodsMicrowave digestion system and hydrogenation atomic fluorescent spectrometry were used in this paper.ResultsLinear range of the method was 0.002 ~ 0.120 mg / L, the recovery was 86.8 ~ 109.6 %, the average recovery was 101.7% with RSD = 1.7%. The determination limit of the method was 0.040 mg / kg.ConclusionThe method possesses the characteristics of convenience, safety, high sensitivity, good precision and accuracy, and it can be used for the determination of total arsenic in Chinese herb. Keywords:MWS; AFS; Poligonum capitatum; Arsenic Polygonum Poligonum capitatum Ham.ex D. Don of Polygonaceae (Polygonaceae) plants, Guizhou Miao people, is widely used in treatment of urinary system diseases, its unique efficacy of urinary tract infections [1], you can heat detoxification, diuretic Tonglin. Therefore, can be used for hot and humid Accumulation, urine yellow red, dripping astringent pain of the disease and urinary tract infections. The drug is currently not found in adverse reactions has been selected as the national medicine protected species in 2002, into the National Essential Drugs