North Calcitum Quality Standard.docVIP

North Calcitum Quality Standard Of: Xia Zhenjiang, Wei Lixin, Du Yuzhi, Xiaoyuan Can, Lu Ping, Dongping, Xia Yang, Li Cen [Abstract] Objective To establish quality standards for the North Calcitum. Methods of chemical identification method of calcium and sulfate North Calcitum the differential response; using acetic acid disodium EDTA Titration with Water in the North Calcitum sulfate calcium (CaSO4 · 2H2O) content. Results disodium ethylene diamine tetraacetate Titration with Water in the North Calcitum calcium sulfate (CaSO4 · 2H2O) content, good repeatability (RSD = 0.24%), calcium sulfate water (CaSO4 · 2H2O) at 0.000 4 ~ 0.249 8 g good linear relationship (r = 0.999 7), the average recovery was 103.95%, RSD = 2.83% (n = 6) .6 batches of samples in the average content of CaSO4 · 2H2O to 98.62%. Conclusion The method of quantitative determination of the North Calcitum simple and accurate, able to control the quality of the mineral drugs. [Keywords:] acetic acid disodium EDTA Titration; North Calcitum Abstract: ObjectiveTo establish the method of quality control for Beihanshuishi. MethodsTo detect calcium salt and sulfate by chemical identification, and to determine the quantity of CaSO4 · 2H2O in Beihanshuishi by Calcium Disodium Versenate coordination titration Method. ResultsThe method for the determination of CaSO4 · 2H2O in Beihanshuishi was in good reproducibility (RSD = 0.24%). The calibration curve was linear (r = 0.999 8) within the reage of 0.000 4 ~ 0.249 8 g of CaSO4 · 2H2O. The recovery was 103.95%, RSD = 2.83%. ConclusionThis method is convenient and accurate, and it can be used to establish quality control of the medicinal material. Keywords:: Calcium Disodium Versenate coordination titration method; Beihanshuishi Calcitum (Gypsum) first appeared in the lt;lt;Wu Pu Materia Medicagt;gt;, as the condensate water stone alias [1]. In ““ China Pharmacopoeiagt; “(2005) prescription formulations taste in 5 North Calcitum used [2] . In o