Qingfei quality standard of fire suppression.docVIP

 PAGE \* MERGEFORMAT 12 Qingfei quality standard of fire suppression Of: Zhang Xiaohui WANG Rui-ming Ni Yan Li Xianrong [Abstract]: Objective To establish a piece of fire suppression Qingfei quality standards. Methods TLC Qingfei tablets in the fire suppression flavescens, Treats, Peucedanum were qualitatively identified, by high performance liquid chromatography prescription baicalin content. Using ODS column, mobile phase: methanol - water - phosphoric acid (47:53:0.2), flow rate: 1 mL / min, column temperature 25 ℃, detection wavelength: 280 nm. The results of this product qualitative characteristics of thin layer chromatography identification of obvious specific, baicalin linear range of 0.163 ~ 0.975 μg, r = 0.999 9, the average recovery rate of 97.43%, RSD = 1.97% (n = 6). Conclusion The method is reproducible, simple, effective control Qingfei fire suppression film quality. [Keywords:] Qingfei fire suppression film before Hu Huangbai flavescens quality standards of baicalin Abstract: Objective To establilsh the quality standard for Qingfei Yihuo tablet. Methods TLC was performed to identify Sophora flavescens Ait, Peucedani and Cortex Phellodendri. HPLC was used to determine Baicalin. ODS column was used. The mobile phase consisted of methanol-water-phosphoric acid (47:53:0.2). The flow rate was 1.0 mL / min and column temperature was at 25 ℃. The detecting wave length was at 280 nm. Results The characteristic for identification by TLC was distinct and hightly specific. Baicalin could be determined by HPLC. The linearity of Baicalin was good in the range of 0.163 ~ 0.975 μg (r = 0.999 9). The average recovery of Baicalin was 97.43% and RSD was 1.97% (n = 6). Conclusion The methods of identification and quantification is simple and reproducible. It can be used effectively for the quality control of Qingfei Yihuo table. Keywords:: Qingfei Yihuo tablet, Sophora flavescens Ait, Peucedani; Cortex Phellodendri; Baicalin, quality standard Qin