Quality Standard of nourishing sedative pills.doc

 PAGE \* MERGEFORMAT 9 Quality Standard of nourishing sedative pills [Abstract] Objective To improve the quality standards nourishing and sedative pills. Methods TLC identification of agents of Millettia, Eclipta, nourishing blood by high performance liquid chromatography Emodin sedative pills. The results of chicken cuneata, Eclipta TLC spots were clear and emodin 0.009 92 ~ 0.124 0 μg range a good linear relationship, the average recovery was 96.2%, RSD = 1.1%. Conclusion TLC and determination methods are simple and easy and repeatable. [Keywords:] nourishing sedative pills, TLC, emodin, high performance liquid chromatography Abstract: Objective To improve the quality standard for Yangxue Anshen Pills. Method TLC was used to identify caulis spatholobi and herba ecliptae, and HPLC to determine the content of emodin. Results The TLC spots of caulis spatholobi and herba ecliptae were clear. The linear range of emodin was 0.009 92 ~ 0.124 0 μg. The average recovery rate was 96.2%, and RSD was 1.1%. Conclusion The methods are simple and accurate, with good reproducity. Keywords:: Yangxue Anshen Pills, TLC, emodin, HPLC Nourishing sedative pills by the Caulis, Millettia, Rehmannia glutinosa, Rehmanniae, Albizia, Eclipta, Agrimony 7 taste medicinal composition, with nourishing Yin, Ning Anshen the effect of [1]. For Less blood deficiency palpitations, dizziness, insomnia, dysphoria heat. the original standard of only microscopic identification items. In order to control quality and ensure safe and effective drug, this study adds Millettia and thin Eclipta Layer Chromatography and high performance liquid chromatography (HPLC) method for the determination of the Caulis emodin. The results show that the method is simple, fast, specific and satisfactory results. An instrument and reagent Shimadzu LC-10A vp HPLC. Emodin (batch number 110756-200110), formononetin (batch number 111703-200501), Millettia control medicine, Eclipta reference drug (Lot 9