Atomic Force and Optical Microscopy Characterization of the Deformation of Individual Carbon Nanotubes and Nanofibers英文文献资料.docVIP

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Atomic Force and Optical Microscopy Characterization of the Deformation of Individual Carbon Nanotubes and Nanofibers英文文献资料.doc

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Atomic Force and Optical Microscopy Characterization of the Deformation of Individual Carbon Nanotubes and Nanofibers英文文献资料

HindawiPublishingCorporation JournalofNanomaterials Volume2008,ArticleID352109,7pages doi:10.1155/2008/352109 ResearchArticle AtomicForceandOpticalMicroscopy CharacterizationoftheDeformationofIndividual CarbonNanotubesandNano?bers TerryP.Bigioni1,2andBrettA.Cruden1 1 2 NASAAmesResearchCenter,UniversityA?liatedResearchCenter(UARC),Mo?ettField,California,CA94035,USA DepartmentofChemistry,TheUniversityofToledo,Toledo,OH43606,USA CorrespondenceshouldbeaddressedtoBrettA.Cruden,brett.a.cruden@ Received4September2007;Revised31December2007;Accepted12January2008 RecommendedbyJunLou Apopulartechniqueforcharacterizingthemechanicalpropertiesofcarbonnanotubesistoapplyaone-dimensionaxialcompres- sionandmeasureitsresponsetothecompressiveforce.Atsomecriticalcompression,adramaticdecreaseintheforceisobserved. ThishaspreviouslybeenattributedtoEulerbuckling,allowingtheelasticmodulustobecalculatedfromtheEulerbucklingforce. Wehaveattachedindividualplasmaenhancedchemicalvapordeposition(PECVD)growncarbonnano?bers(CNFs)andthermal chemicalvapordeposition(CVD)growncarbonnanotubes(CNTs)totheapexofanatomicforcemicroscope(AFM)cantilever toexaminethismechanicalresponse.Bycombiningtheforcemeasurementsandsimultaneousvideomicroscopy,weareableto observethemechanicaldeformationandcorrelatepointsintheforcecurvewithphenomenasuchasslippingandbending.Anal- ysisofthemechanicalresponsemustthereforebeinterpretedintermsofbendingand/orslippingofatubecompressedbyan o?-normalforce. Copyright?2008T.P.BigioniandB.A.Cruden. This is an open access article distributed under the Creative Commons AttributionLicense,whichpermitsunrestricteduse,distribution,andreproductioninanymedium,providedtheoriginalworkis properlycited. 1. INTRODUCTION crease[10,11].Avariationonthecarbonnanotube,often calledacarbonnano?ber(CNF),whichisgrownbyplasma enhancedchemicalvapordeposition(PECVD),shouldshow asigni?cantreductioninmodulusrelativetotheCNTdueto itsstackedconegraphenemorphology[12].StilltheCNFis ofinterestasitmaybegrownasafree