Blue-Emitting Small Silica Particles Incorporating ZnSe-Based Nanocrystals Prepared by Reverse Micelle Method英文文献资料.docVIP

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Blue-Emitting Small Silica Particles Incorporating ZnSe-Based Nanocrystals Prepared by Reverse Micelle Method英文文献资料.doc

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Blue-Emitting Small Silica Particles Incorporating ZnSe-Based Nanocrystals Prepared by Reverse Micelle Method英文文献资料

HindawiPublishingCorporation JournalofBiomedicineandBiotechnology Volume2007,ArticleID52971,6pages doi:10.1155/2007/52971 ResearchArticle Blue-EmittingSmallSilicaParticlesIncorporatingZnSe-Based NanocrystalsPreparedbyReverseMicelleMethod MasanoriAndo,ChunliangLi,PingYang,andNorioMurase PhotonicsResearchInstitute,NationalInstituteofAdvancedIndustrialScienceandTechnology(AIST),KansaiCenter, 1-8-31Midorigaoka,Ikeda563-8577,Osaka,Japan CorrespondenceshouldbeaddressedtoNorioMurase,n-murase@aist.go.jp Received16May2007;Revised17December2007;Accepted24December2007 RecommendedbyMarekOsinski ZnSe-basednanocrystals(ca.4-5nmindiameter)emittinginblueregion(ca.445nm)wereincorporatedinsphericalsmallsilica particles(20–40nmindiameter)byareversemicellemethod.Duringthepreparation,alkalinesolutionwasusedtodepositthe hydrolyzedalkoxideonthesurfaceofnanocrystals.ItwascruciallyimportantforthissolutiontoincludeZn 2+ ionsandsurfactant molecules(thioglycolicacid)topreservethespectralpropertiesofthe?nalsilicaparticles.Thisisbecausethesesubstancesinthe solutionpreventthesurfaceofnanocrystalsfromdeteriorationbydissolutionduringprocessing.Theresultantsilicaparticleshave anemissione?ciencyof16%withmaintainingthephotoluminescentspectralwidthandpeakwavelengthoftheinitialcolloidal solution. Copyright?2007MasanoriAndoetal. This is an open access article distributed under the Creative Commons Attribution License,whichpermitsunrestricteduse,distribution,andreproductioninanymedium,providedtheoriginalworkisproperly cited. 1. INTRODUCTION transition.ThisslowdecaycausesthesaturationofPLinten- sitywhentheexcitationlightintensityisincreased. Developmentofbrightandstablephosphorsisincreasingly requiredinmany?elds.TheII-VIsemiconductornanocrys- tals (NCs) such as ZnSe and CdTe attract much interest asnovelbrightphosphorswithtunablephotoluminescence (PL)wavelength[1]forpossibleusesincludingbiologicalla- beling[2–6],display,andlightingdevices[7–9].Forbiolog- icallabeling,?uorophoresareboundtobiologicalmole