模板法室温制备纳米CeO2及其表征.pdfVIP

模板法室温制备纳米CeOz及其表征／胡震 · 67· 模板法室温制备纳米Ce02及其表征 胡 震 (四川理工学院材料与化学工程系，自贡643000) 摘要 用下制备纳米Ce02粉体材料。采用傅立叶变换红外光谱仪、X射线衍射仪、差热一热重联用分析仪、扫描电镜、紫外一 可见分光光度计和紫外发射光谱仪分别对所制备的产物进行表征。结果表明：所制备的ceOz粒径为15nm，热稳定 性好，属于萤石结构，分散性好，对紫外光具有较好的吸收，对可见光具有较好的透明性，纳米ce02粉体的纯度大于 99．5％。该制备方法具有工艺简单、污染少、粒径小和操作可控等优点。 关键词 模板法纳米Ce02表征 中图分类号：0611．61 文献标识码：A The ofNanometer Routeat Preparation Ce02 byTemplate Ambient andItsCharacterization Temperature HUZhen ofMaterialandChemical of (Department Engineering，SichuanUniversity 643000) AbstractInthis work，nanometerCe02 are a route．Thematerialsincludsce— particlespreparedbytemplate rium and sulfatesodium thesurfactantis alcohol(PVA)whichand the hydroxide，and polyvinyl dispersesprotectsprod— are Fr-IR uct．The characterized andTGA-DTAinstruments，SEM，theUV—VIS products by spectrum，XRD speetro— 756MCandultravioletemission instruments．Theshowthatthe sizeis photometer spectrograph experiments particle about thermal is it 15nm，the is structureisformed，andhaveex- stabilityverygood，dispersiongood，fluoritesystem cellent inUV and inthe is visible thanor absorptioncapabilityrayregionhightransparency region．The