核壳结构型Fe3O4@C@mSiO2复合物制备.docVIP

核壳结构型Fe3O4@C@mSiO2复合物制备 　　【摘 要】本文通过溶剂热法制备了粒径较均匀的磁性 Fe3O4 粒子，后利用喷雾干燥技术在其表面包覆了一层碳，采用溶胶―凝胶过程在碳层上包覆一层介孔结构的氧化硅，得到了磁性核/介孔壳结构的复合材料。氮气吸附脱附测试显示所得复合材料具有较高的孔容和比表面积 【关键词】核壳结构；磁性材料；四氧化三铁；介孔氧化硅；碳材料 【Abstract】Solvothermal？method was adopted to prepare uniform Fe3O4 magnetic nanoparticles.Then Carbon was deposited on Fe3O4 by spray-drying process.Mesoporous silica was deposited on the Fe3O4 core by sol-gel method.Core-shell structured magnetic mesoporous composites was obtained.The results showed that the composites possess relatively large pore volume and specific surface area. 【Key words】Core-shell