注射用盐酸头孢甲肟含量测定及有关物质检查方法的研究论文.docVIP

　　注射用盐酸头孢甲肟含量测定及有关物质检查方法的研究论文 .freelm×4.6mm，5μm)色谱柱，流动相采用水∶冰乙酸∶乙腈(850∶17∶150)，流速1.0ml/min，检测波长254nm。结果 溶液浓度在0.06～500μg/ml范围内线性良好，r=0.9997(n=12)，方法平均回收率为99.87%，RSD为0.36%(n=9)。盐酸头孢甲肟杂质数目为14至15个.freelination of cefmenoxime hydrochloride for injection ABSTRACT Objective To develop a method for the determination of cefmenoxime hydrochloride for injection and it′s related substances by HPLC. Method Samples n obile phase of l/min and detection . Result The standard curves l (r=0.9997). The average recovary ber of related substances in cefmenoxime hydrochloride is 14～15 and the total amount is 1.00%