以豆腐柴叶为原料提取果胶工艺研究.pdfVIP

天然产物研究与开发 Nat Prod Res Dev，20o7，19：480-485 文章编号：1001-6880(2007)Suppl-0480-06 以豆腐柴叶为原料提取果胶工艺研究 王存文h，王为国 ，吴元欣 ，池汝安 ，张俊锋 ，徐 汶 ‘武汉工程大学湖北省新型反应器与绿色化学工艺重点实验室； 武汉工程大学化工与制药学院，湖北430074 摘 要：本文开发了一条从豆腐柴叶中提取果胶的新工艺。该工艺中，树脂吸附纯化、超滤浓缩和喷雾干燥是 三个重要的单元操作。为了确定最佳提取条件和考察树脂吸附纯化和超滤浓缩两个单元操作的商业应用可行 性，进行了三种不同规模的试验。结果表明，所开发的工艺在能耗和果胶质量方面明显优于传统的醇沉淀法。 关键词：豆腐柴；提取；果胶；树脂吸附；超滤 中图分类号：R284．2 文献标识码：A WANG Cun—wen ’，WANG Wei—guo ，WU Yuan．xin ，CHI Ru．an ，ZHANG Jun．feng ，XU Wen Hubei Key Laboratory ofNovel Reacmr and Green Chemical Technology； School ofChemical Engineering and Pharmacy，Wuhan Institute ofChemical Technology，Hubei 430074，China Abstract：A technology for extracting pectin from leaves of Premna subscandens has been developed．In the process，three main unit operations play key role，which are resin adsorption purification，ultra—filtration and spray dry．Three different scale expefimenm were carried out so as to determine the optimum extracting conditions and to examine the commercial feasibility of two unit operations of the resin adsorption purification and the ultra—fihration，respectively．The experimental results showed that the developed process is better than that of the traditional alcohol precipitation in term of energy-·PA)n—- serve and pectin quali~． Key words：Premna subscandens；extraction；pectin；resin adsorption；ultra—filtration novel technologies for pectin preparation． The traditional process consists mainly of a serial of u— Pectin is an important constituent substance inside cell nit operations，including acid ext