液相色谱操作规程（Liquid chromatography operating procedures）.docVIP

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液相色谱操作规程（Liquid chromatography operating procedures）.doc

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液相色谱操作规程（Liquid chromatography operating procedures） First, turn on the computer Two, open the host, preheat Three, enter the instrument workstation, on-line, and set the instrument using methods and instrument parameters Four, start the pump power system pretreatment (exhaust, etc.) Five, check whether the liquid column pressure is normal Six 、 setting up the instrument method, including the use condition of the instrument, etc. Seven, activate the operation method, wait for instrument balance, the baseline is straight Eight, after the instrument Ready, can carry on the sample analysis Nine, after the operation test, clean all the experimental materials, do a good job cleaning Ten. Record the use of logs and check with the administrator Matters needing attention I. the flow of high performance liquid chromatography adopts chromatographic pure solvent to meet the requirements of the instrument and avoid damaging the chromatographic column; Two, prohibit the use of contaminated water and other washing chromatography column, to avoid the solvent with each other into the pump; Three. The mobile phase can be used after filtration and degassing; Four. The sample to be analyzed must be thoroughly dissolved, clarified and filtered to avoid clogging and damage to the chromatographic column; Five. After analysis, attention should be paid to cleaning the colorimetric column and the colorimetric cell of the detector in time. Operation regulation of SHIMADZU LC-10AD high performance liquid chromatograph 1. purpose To standardize the use of SHIMADZU LC-10AD high performance liquid chromatography (HPLC). 2. range The utility model is suitable for the use of SHIMADZU LC-10AD type high performance liquid chromatograph. 3. responsibilities The inspector is responsible for implementing this regulation. 4. rules 4.1 system composition This system is composed of 1 LC-10ADvp solvent pump, FCV-10AL low pressure gradient mixer, in-line degasser, Rheodyne 7725i manual injection valve, SPD-