原创力文档developed new procedure for low concentrations of hydrazine determination by spectrophotometry hydrazine-potassium permanganate system开发新程序,低浓度的测定肼分光光度法hydrazine-potassium高锰酸盐体系.pdfVIP
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developed new procedure for low concentrations of hydrazine determination by spectrophotometry hydrazine-potassium permanganate system开发新程序,低浓度的测定肼分光光度法hydrazine-potassium高锰酸盐体系
Journal of Analytical Sciences, Methods and Instrumentation, 2012, 2, 98-102
/10.4236/jasmi.2012.22018 Published Online June 2012 (http://www.SciRP.org/journal/jasmi)
Developed New Procedure for Low Concentrations of
Hydrazine Determination by Spectrophotometry:
Hydrazine-Potassium Permanganate System
1 2 1 1 1 1
S. Ganesh , Fahmida Khan , M. K. Ahmed , P. Velavendan , N. K. Pandey , U. Kamachi Mudali
1Reprocessing Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, India; 2Department of Chemistry, National Institute of
Technology, Raipur, India.
Email: fkhan.chy@nitrr.ac.in
Received October 12th, 2011; revised November 23rd, 2011; accepted January 9th, 2012
ABSTRACT
An indirect, sensitive and accurate method for the determination of trace amounts of hydrazine is described. In this
proposed the spectrophotometric method is based on its reduction properties of hydrazine with a known concentration
of potassium permanganate to reduce the colour. The absorbance of unreduced permanganate is measured the colour
difference at different wavelengths 546 and 526 nm which show an absorption spectrum with hydrazine. Hydrazine can
be determined in the range of 100 - 700 µg/ml with correlation coefficient of 0.999 and relative standard deviation 1%.
The method is successfully applied for the determination of hydrazine in water streams in nuclear reactors/purex proc-
ess/boiler water and polluted water samples.
Keywords: Hydrazine/Potassium Permanganate; UV-Vis Spectrophotometry; Reducing Property; Water Streams;
Nuclear Reactors
1. Introduction spectrophotometric procedure for the determination of
ppm concentrations of hydrazine salts based
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