effect of the preparation method on coal2o3 catalyst applied to ethanol steam reforming reaction production of hydrogen影响coal2o3催化剂的制备方法应用于乙醇水蒸气重整反应生产氢.pdfVIP

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effect of the preparation method on coal2o3 catalyst applied to ethanol steam reforming reaction production of hydrogen影响coal2o3催化剂的制备方法应用于乙醇水蒸气重整反应生产氢.pdf

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effect of the preparation method on coal2o3 catalyst applied to ethanol steam reforming reaction production of hydrogen影响coal2o3催化剂的制备方法应用于乙醇水蒸气重整反应生产氢

Modern Research in Catalysis, 2012, 1, 52-57 /10.4236/mrc.2012.13007 Published Online October 2012 (http://www.SciRP.org/journal/mrc) Effect of the Preparation Method on Co/Al O Catalyst 2 3 Applied to Ethanol Steam Reforming Reaction Production of Hydrogen Silmara Rodrigues Garcia, José Mansur Assaf Laboratory of Catalysis-Chemical Engineering Department, Federal University of Sao Carlos, São Carlos, Brazil Email: silmararodriguesgarcia@ Received August 29, 2012; revised September 30, 2012; accepted October 8, 2012 ABSTRACT Alumina supported cobalt catalysts were prepared, characterized and applied in ethanol steam reforming for hydrogen production. The support and the supported catalysts were prepared, respectively, by the solvothermal and precipitation, impregnation and deposition-precipitation methods. The cobalt was added by impregnation and deposition-precipitation in the Al O supports using a Co(NO ) ·6H O solution. The solids were characterized, Temperature-Programmed Re- 2 3 3 2 2 duction with H (RTP-H ), X-Ray Diffraction (DRX), BET Nitrogen Adsorption and Temperature Programmed Oxida- 2 2 tion (TPO). The results indicated that the preparation method and the treatment conditions of samples were appropriate for obtaining the wanted compounds. Co O phase was verified for all catalysts through analyses of DRX and RTP-H 3 4 2 results. Catalytic te