synthesis and evaluation of highly tolerant pd electrocatalysts as cathodes in direct ethylene glycol fuel cells (degfc)合成和评估pd高度宽容electrocatalysts在乙二醇直接燃料电池阴极(degfc).pdfVIP

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synthesis and evaluation of highly tolerant pd electrocatalysts as cathodes in direct ethylene glycol fuel cells (degfc)合成和评估pd高度宽容electrocatalysts在乙二醇直接燃料电池阴极(degfc).pdf

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synthesis and evaluation of highly tolerant pd electrocatalysts as cathodes in direct ethylene glycol fuel cells (degfc)合成和评估pd高度宽容electrocatalysts在乙二醇直接燃料电池阴极(degfc)

Energies 2009, 2, 944-956; doi:10.3390/e OPEN ACCESS energies ISSN 1996-1073 /journal/energies Article Synthesis and Evaluation of Highly Tolerant Pd Electrocatalysts as Cathodes in Direct Ethylene Glycol Fuel Cells (DEGFC) Francisco Javier Rodríguez Varela 1,*, Sergio Fraire Luna 1 and Oumarou Savadogo 2 1 Grupo de Recursos Naturales y Energéticos, Cinvestav Unidad Saltillo, Carr. Saltillo-Monterrey Km. 13.5, Ramos Arizpe, Coahuila, C.P. 25900, Mexico 2 Laboratoire dÉlectrochimie et de Matériaux Énergétiques, École Polytechnique de Montréal, C.P. 6079, succ. Centre-Ville, Montréal, QC, H3C 3A7, Canada * Author to whom correspondence should be addressed; E-Mail: javier.varela@.mx; Tel.: +52-844-438-9612; Fax: +52-844-438-9610. Received: 29 July 2009 / Accepted: 11 September 2009 / Published: 27 October 2009 Abstract: Highly selective Pd electrocatalysts were synthesized by the formic acid (FA) method and evaluated as cathodes for DEGFC applications. In rotating disc measurements in acid medium, the Pd/C cathode showed important catalytic activity for the Oxygen Reduction Reaction (ORR). In the presence of ethylene glycol (EG, C H O ), Pd/C 2 6 2 exhibited a noteworthy electrochemical behavior and full tolerance to the organic molecule.