原创力文档use of a deuterated internal standard with pyrolysis-gcms dimeric marker analysis to quantify tire tread particles in the environment使用氘内部标准pyrolysis-gcms二聚的标记分析量化车轮踏面粒子在环境中.pdfVIP
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use of a deuterated internal standard with pyrolysis-gcms dimeric marker analysis to quantify tire tread particles in the environment使用氘内部标准pyrolysis-gcms二聚的标记分析量化车轮踏面粒子在环境中
Int. J. Environ. Res. Public Health 2012, 9, 4033-4055; doi:10.3390/ijerph9114033
OPEN ACCESS
International Journal of
Environmental Research and
Public Health
ISSN 1660-4601
/journal/ijerph
Article
Use of a Deuterated Internal Standard with Pyrolysis-GC/MS
Dimeric Marker Analysis to Quantify Tire Tread Particles in
the Environment
Kenneth M. Unice *, Marisa L. Kreider and Julie M. Panko
ChemRisk LLC, Pittsburgh, PA 15222, USA; E-Mails: mkreider@ (M.L.K.);
jpanko@ (J.M.P.)
* Author to whom correspondence should be addressed; E-Mail: kunice@;
Tel.: +1-412-281-6900; Fax: +1-412-281-6999.
Received : 21 September 2012; in revised form : 22 October 2012 / Accepted : 31 October 2012 /
Published : 8 November 2012
Abstract: Pyrolysis(pyr)-GC/MS analysis of characteristic thermal decomposition fragments
has been previously used for qualitative fingerprinting of organic sources in environmental
samples. A quantitative pyr-GC/MS method based on characteristic tire polymer pyrolysis
products was developed for tread particle quantification in environmental matrices
including soil, sediment, and air. The feasibility of quantitative pyr-GC/MS analysis of
tread was confirmed in a method evaluation study using artificial soil spiked with known
amounts of cryogenically generated tread. Tread concentration determined
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