原创力文档超高效液相色谱-串联质谱法测定鸡组织和牛组织中的甲苄喹啉和癸氧喹酯 determination of nequinate and decoquinate residues in chicken tissues and bovine tissues by ultra performance liquid chromatography-tandem mass spectrometry.pdfVIP
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超高效液相色谱-串联质谱法测定鸡组织和牛组织中的甲苄喹啉和癸氧喹酯 determination of nequinate and decoquinate residues in chicken tissues and bovine tissues by ultra performance liquid chromatography-tandem mass spectrometry
5 11 Vol. 5 No. 11
2014 11 Journal of Food Safety and Quality Nov. , 2014
-
*
林 黎, 康海宁 , 肖陈贵, 沈金灿, 叶 刚
( , 518045)
摘 要: 目的 -
方法 , -(hydrophile-lipophile balance, HLB) ,
-, 结果 0.005~0.250 mg/ kg
, 0.999, 0.01 mg/kg, 77.0%~110%,
1.36%~12.4%结论 ,
关键词: ; ; -; ;
Determination of nequinate and decoquinate residues in chicken tissues and
bovine tissues by ultra performance liquid chromatography-tandem
mass spectrometry
*
LIN Li, KANG Hai-Ning , XIAO Chen-Gui, SHEN Jin-Can, YE Gang
(Key Laboratory of Detection Technology R D on Food Safety , Food Inspection and Quarantine Center, Shenzhen
Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518045, China)
ABSTRACT: Objective To develop a method for determination of nequinate and decoquinate residues in
chicken tissues and bovine tissues by ultra performance liquid chromatography-tandem mass spectrometry
(UPLC-MS/MS). Methods The residues of nequinate and decoquinate in the test sample were extracted with
acetonitrile. The extraction was cleaned with hydrophile-lipophile balance (HLB) cartridge. The residues were
de
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