热压加工对含Mn块体纳米晶Fe3Al组织和性能的影响.PDFVIP

2 0 0 9 中国铸造活动周论文集 热压加工对含Mn 块体纳米晶 Fe Al 组织和性能的影响 3 喇培清,李玉峰,路 阳 （兰州理工大学 甘肃省有色金属新材料国家重点实验室培育基地，甘肃 兰州 730050） 摘要：:对通过铝热反应熔化制备的含Mn 10%块体纳米晶Fe Al 材料在不同温度、不同次数下进行了 3 热压加工，利用XRD 研究了热压加工前后纳米晶粒尺寸的变化，并测试了硬度变化和压缩率。结果 显示，热压加工后晶粒尺寸都发生了增大。在同一温度下，随着热压次数的增加，晶粒尺寸逐渐减 小，在同一压次下，晶粒尺寸随着热压温度升高而增大；在 800℃时，材料的硬度随热压次数增加 而减小，在热压加工 5 次时，随着热压加工温度的升高，材料的硬度逐渐增大；热压加工后的纳米 晶晶粒尺寸和硬度符合反常的Hall-Petch 关系；热压加工 ，材料表现出良好的塑性变形，并随着 温度升高和压次增大，材料压缩率增大，当热压加工温度为1000℃时，热压次数对压缩率的影响变 化不大。 关键词：:热压加工; 纳米晶Fe Al; 晶粒尺寸; 硬度; 压缩率 3 Effect of hot processing on the microstructure and mechanical properties of the bulk nanocrystalline Fe Alwhich contains Mn element 3 LA Pei-qing, LI Yu-feng, LU Yang （State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology，Lanzhou 730050 ，China ） Abstract Different temperatures and times of the hot processing of the bulk nanocrystalline made by aluminothermic reaction；the grain size is investigated by XRD, and the hardness, compression ratio were also measured. The results show that the grain size increased after hot processing, In identity temperature, the grain size decreased with the increasing times of the hot processing and In identity times of hot pressing, the grain size increased with the increasing temperature of the hot processing; The hardness decreased with the increasing times of the hot processing at 800 ℃; The hardness increased with the increasing temperature of the hot processing ;The grain size and hardness of the nanocrystalline after hot processing are contrary to the Hall-Petch relation; The materials have a g