气雾化法制备Fe-6.5%Si-x%Ni合金粉末及其性能的研究.doc

气雾化法制备Fe-6. 5%Si-x%Ni合金粉 末及其性能的研究 王山山组强赵鈕姐赵文东刘英杰 北京康普锡威科技有限公司 采用气雾化法制得了 Fe-6. 5%Si-x%Ni (x=0, 0. 2, 0. 5, 0. 8，1.0;质量分数)金 属软磁合金粉末，对合金粉末进行绝缘包覆处理后压制成磁粉芯进行磁性能检 测，磁粉芯尺寸为27 mmX15 mmX5酮，压制压力为1 GPa。利用激光粒度分析 仪、扫描电子显微镜(SEM)、X射线衍射仪(XRD)和软磁交流分析仪对粉末的 粒度分布、形貌、相组成和磁性能进行检测和分析。结果表明:在雾化过程中，随 着Ni元素添加量的增加，金属液粘度增加，雾化时间变长，粉末颗粒尺寸增大， 中位径d50从21. 04 um增大到38. 62 u m;粉末为球形或近球形，部分粉末表而 有卫星球;粉末为单相ci-Fe相，表明Ni元素以固溶体形式溶入基体晶格，造成 晶格畸变，增加了合金粉末的内应力；随着Ni元素含量的升高，矫顽力先升高 后降低，添加1. 0%Ni吋为最优值307. 9 A ? m-1 (0. 05 T，100 k Hz),振幅磁 导率先降低后升高添加1.0%Ni时为最优值15.7 (0.05T，100 k Hz),且在频 率达到80 k Hz时略有升高，磁损耗先升高后降低，在添加1. 0%Ni时为最优值 4595 m W ? cm-3 (0. 05 T，100 k Hz)。 关键词： 气雾化;金属软磁;合金粉末;磁损耗; .?王山山(1989-),男，河北沧州人，研究生，研究方向:气雾化 制粉及其粉末磁性能研宄;E-mail:wangshanl9901221@163. com; 胡强，教授；电话E-mail: hqbpu@263.net 2016-03-14 基金：北京市科技新星计划项目(7141103001814079)资助 Performance Characterization of Gas-Atomized Fe-6. 5%Si-x%Ni Powders Wang Shanshan Hu Qiang Zhao Xinming Sheng Yanwei Zhao Wendong Liu Yingjie Beijing COMPO Advanced Technology Co.，Ltd.; Abstract： Fe~6. 5% Si~x%Ni ( x = 0, 0. 2, 0. 5, 0. 8, 1. 0; mass fraction) soft magnetic alloy powders were produced by gas atomization technology and pressed into magnetic cores for magnetic properties detection. The size of the cores was 27 mm X 15 mm X 5 mm and the pressing pressure was 1 GPa. Laser particle size analyzer, scanning electron microscopy ( SEM) ， X-ray diffraction ( XRD) and soft magnetic AC analyzer were used to detect and analyze the particle size diffraction, morphology, phase composition and magnetic properties. The results showed that， in the process of atomization, the atomization time increased with the increase of the amount of Ni addition due to the improvement of viscosity of the alloy. And the particle size increased with the increase of the amount of Ni addi tion, and the median diameter increased from 21. 04 to 38. 62 u m. The powders were smooth and spherical in shape with a few satellite balls cladded to the surface, a -Fe diffraction peaks were the single p