有机溶剂水热法制备阻燃球形氢氧化镁.PDFVIP

无机盐工业 第 38卷第 3期 40 INORGAN IC CHEM ICALS INDU STRY 2006年 3月 ) 1 2 3 , , ( 1. , 524048; 2. ; 3. ) : , , , XRD, SEM, TEM , , , , , , , , 35% 190 e 5 h , : ; ; ; : TQ 132. 2 : A : 1006 - 4990( 2006) 03 - 0040 - 03 Th e p repara tion of flam e - re tard sph ere cry sta lline m agnesium hyd roxid e b y organ ic solven t- h ydrotherm a l m e th od 1 2 3 W u Ji nsong , L iC ihu , L iH mi in ( 1. L if e Sciences and Chemistry Institute of Zhanj iangN ormal College, Guangdong Zhanj iang 524048, China; 2. The First igh School in Wuchuan City of Guangdong Prov ince; 3. Qinghai Institute of SaltLakes, ChineseA cademy of Sciences) A bstract: T k ing bischofite m ixture in Q ingh i Dongt i s lt l kes s r w m teri ,l sod ium hydrox ide cont in ing cert in of org n ic solvent s precip it tor, the sphere cryst lline m gnesium hydrox ide is syn thesized by reverse precipit tion m ethod in the u tocl ve. The property nd sh pe of the product re ch r cterized by XRD, SEM nd TEM etc. . The resu lts show th t the product is sphere p rt icle w ith un iform distribu tion, w ell d ispersion nd h igh purity. The m ethod c n not on ly smi p lify the process, but lso decre se the production cost, nd further industri l sc ling - up becom es possib le. The in fluences of the content of org nic so lvent in the re ction system, hydrotherm l tem per ture nd tmi e on the sh pe of m gnesium hydrox ide cryst l re stud ied. W hen the re ction system cont ins 35% org n ic solvent, hydrotherm l temper ture