基于芯能级x射线谱学的碳纳米材料的电子结构分析-electronic structure analysis of carbon nano-materials based on core energy level x - ray spectroscopy.docxVIP

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基于芯能级x射线谱学的碳纳米材料的电子结构分析-electronic structure analysis of carbon nano-materials based on core energy level x - ray spectroscopy.docx

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基于芯能级x射线谱学的碳纳米材料的电子结构分析-electronic structure analysis of carbon nano-materials based on core energy level x - ray spectroscopy

The Electronic Structure Investigation of Carbon-based Nanomaterials by Core Level Spectrascopy Abstract A comparative XAS study of the MnOx@GO composite with different component has been performed. The XAS results clearly indicate the oxidation state of Mn and chemical information for the MnOx@GO, which synthesized by different ratio of graphite and KMnO4. When graphite/KMnO4 ratio was less than 1:2, Mn shows the Mn4+. Mn2+ or Mn3+ existed in the composite when the ratio was more than 1:1. XAS and XES have been applied into interaction between the RGO and Fe3O4 in RGO-Fe3O4 composite for the anode materials of lithium ion battery. Meanwhile, the fade of capacity have been investigated by the comparative XAS and XES study of the anode materials in different cycles. It could be that the interaction becomes weaker after several cycles. Key words: Carbon nanocages, graphene-metal oxide composite, N doping, core-level X-ray spectroscopy. Written by Hui Zhang Supervised by Prof. Xuhui Sun V 目录 HYPERLINK \l _bookmark0 第一章碳纳米材料概述 ······································································· 1 HYPERLINK \l _bookmark1 1.1 从碳纳米管到碳纳米笼 ····························································· 1 HYPERLINK \l _bookmark4 1.1.1 碳纳米笼的合成 ······························································ 3 HYPERLINK \l _bookmark8 1.1.2 碳纳米笼的应用 ······························································ 5 HYPERLINK \l _bookmark12 1.2 石墨烯··················································································· 8 HYPERLINK \l _bookmark14 1.2.1 石墨烯在电化学领域中的应用 ············································ 9 HYPERLINK \l _bookmark18 1.3 本论文的研究内容和意义 ·············································??··········· 13 HYPERLINK \l _bookmark19 第二章纳米研究中的芯能级 X 射线谱学 ················································ 14 HYPERLINK \l _bookmark20 2.1 基本介绍··············································································· 14 HYP