不同产地白芷的质量分析和提取工艺优化-quality analysis and extraction process optimization of angelica dahurica from different areas.docxVIP

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不同产地白芷的质量分析和提取工艺优化-quality analysis and extraction process optimization of angelica dahurica from different areas.docx

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不同产地白芷的质量分析和提取工艺优化-quality analysis and extraction process optimization of angelica dahurica from different areas

量为 147.32mL；异欧前胡素的最佳提取工艺为甲醇浓度 91.83%，提取时间为 9.15h，甲醇用量为 112.68mL。关键词：白芷；欧前胡素；异欧前胡素；质量研究；微量元素；星点设计ABSTRACTObjective: Pass the analysis to different Angelicadahurica ( Fisch.ex Hoffm.)Benth.etHook.F quality in the habitat, as to its do an objective evaluation, provide for the Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F quality evaluation certain basis; Then to the content comparison of Imperatorin and Isoimperatorin that different habitat Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F contains, for of the effective composition analysis provide a basis. Make use of Atomic Absorption Spectrophotometry to measurese in the middle of Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F a few contents of trace elements counteract Systematic Cluster Analysis method as to its carry on analysis, combined it to carry on first step with the relativity of Chinese herbal medicine curative effect study, provide for the research of trace element in Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F a basis.application Central Composite of Response Surface, excellent turn a withdrawing of Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F craft condition.Method: To the sex form of different habitat Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F, show minute details a characteristic, thin layer characteristic, physics and chemistry characteristic and ether to immerse a thing, total ash cent content and humidity content and the content of Imperatorin and Isoimperatorin to carry on a comparison research. Use the difference of more different trace element content of Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F in the habitat of Systematic Cluster Analysis method, application Central Composite of Response Surface method is excellent to turn an Angelicadahurica ( Fisch.ex Hoffm.)Benth.et Hook.F reflux to withdraw a craft.Result and conclusion: Carry on the powder characteristic that shows minute details the observation detection different sample to the Angelicadahurica (