反应烧结制备alnsic复合材料工艺分析-technological analysis of aln sic composite prepared by reaction sintering.docxVIP

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反应烧结制备alnsic复合材料工艺分析-technological analysis of aln sic composite prepared by reaction sintering.docx

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反应烧结制备alnsic复合材料工艺分析-technological analysis of aln sic composite prepared by reaction sintering

AbstractWithaluminumpowder,siliconnitridepowderandcarbonblackastherawmaterials,AlN-SiCsolidsolutionwassynthesizedbyin-situchemicalsynthesisinvacuumatmosphereat1850℃for1.5hwhilethepre-AlNtechnologywereinvestigatedinthissystem.Theexperimentwasdesignedtocomparethecompressiontestatlowtemperatureof450℃andhightemperatureof1850℃.ObservingandanglicizingbyXRDandSEM,itcomparestheresultsoftwohot-presstechnology.Itstudiespre-pressurizedtemperatureofAlN,aswellastheimpactofaproduct.Throughthedesignandexperimentaldemonstration,theinitialloadingprocessatlowtemperaturecansignificantlyimprovethelevelofdensedegreeofthecompositematerialssoastoeffectivelyincreasetheflexuralstrengthofAlN-SiCceramiccompositespreparedbyin-situreaction,whilefracturetoughnessisntinobviousregularity.Basedontheidentification,duringtheprocessofsinteringofmaterialsinthissystem,loadingatlow-temperaturecaneffectivelyusethelow-temperatureplasticnatureofactivefillerAltoreachapreliminarydensenesssoastoimprovethedensedegreeofthefinalproduct.Inacertaindensity,thefinalproductsconfigurationdeterminesthefracturetoughnessofmaterialsinthissystem.Atthesametime,comparedwiththeresultswhensinteringmaterialofsamesystemunderthenon-pressurevacuumatthesametemperature,theAlN-SiCceramiccompositespreparedbythehotpressingprocessshowamorereasonablemechanicalproperties,withtheflexuralstrengthreaching560MPa±20MPa,Vickershardnessofpolishingsurfacereaching2.2GPa,andthefracturetoughnessKIcreaching3.76±0.3MPa·m1/2.ThemechanismsofreactionofAl,C(carbonblack)andSi3N4throughhightemperaturewerediscussedbydesigningaseriesofheatingtemperature.ThereationroutesofAl,C(carbonblack)andSi3N4with3wt%additiveofY2O3wereinferredbyXRDanalysis.WiththemeltingofAl,thereactionoftherawmaterialsystemwastriggedthroughAl4C3.Simultaneously,thereactionsinteringprograssshowedthatthecomformationtheframeworkofthematrixtookplacealongwiththereactionproceeding.AndtheextraAlNmixedwithrawmaterialbeforehandcouldadjusttherelativedensityoftheproductsbasedonthethereactionsinteringm