特殊形貌无机资料的水热合成.pdfVIP

摘 要 本论文袋周水热方法避行具有特殊形貌的钒酸鹱晶体的合成 磺究王号筝，初步探索具寄特殊形貌过渡金属豹钒酸黧晶俸瀚合成 规律，找毖合成避稳中的影响函素，开发过渡金耩钒酸赫的低淀 合成路线，合成其有橹豫形虢静锈羧艋酌攀菇，有秘予菠袋薪稀 耱。 专A文王俘弱蓬点富强个方嚣，～是礤突了过渡金属键羧盐的 台或趣臻，找翻了会袋过程中麴影响飘素，对以后鞠合成其有一 定的搬导意义，二怒样品静含成，在Li20一ZnO．V205．H20体系中 合成了熬有辫歇结稳的薪物栩和其稳死姆过渡众藕密鼋镳酸盐肇 菇，并对群菇进行了IR、SEM、XRD蠢嚣DS表强。 论文工{髻表弱承菸方法怒一条台戏具囊特球形貔镊羧慧兹有 效途臻。透适合理懿调节爱应魏酝毙、调节髂系约PH焦、选撵 含透的反应滠度，可以褥到具窍管状维构的钒酸盐鼷体。 关键谲：过渡金属；承滚食成：锍惹能合物；SEM、lR、XRD、EDS 表蔹 Abstract vanadateswith were The metal transition specialmorphology the atlow synthesizedby hydrothermaltechniquetemperature，and characterized andEDS bySEM，XRD，IR technique．The for ofthe the transition and factors synthesis affecting regulations with wereobtainedandthe metalvanadates specialmorphology of was routelow synthesisdeveloped． temperature were tothe oftransitionmetal Mostattentions payed synthesis transition vanadates．Theofthe metalvanadiumoxide regulations werefound．Thoseresultsare to the synthesis helpfulsynthesize vanadates Zincvanadate with effectively， crystals tubular were andcharacterized synthesized SEM，IR，XRD morphology by andEDS， Someresultscanbemadeformthestudy．Hydrothermal aneffective the is routef