白钨矿酸分解萃取制取磷钨杂多酸盐工艺分析-technological analysis of phosphotungstic heteropoly acid salt prepared by acid decomposition and extraction of scheelite.docxVIP

3.1实验部分........................................................................................................................173.1.1实验试剂..............................................................................................................173.1.2实验仪器及设备..................................................................................................173.1.3实验装置及操作步骤..........................................................................................173.1.4检测方法..............................................................................................................183.2实验结果与讨论............................................................................................................183.2.1搅拌速度的影响..................................................................................................183.2.2盐酸初始浓度的影响..........................................................................................193.2.3磷酸用量的影响..................................................................................................213.2.4反应温度的影响..................................................................................................243.2.5活化能的求取......................................................................................................263.2.6宏观动力学方程的建立......................................................................................273.3本章小结........................................................................................................................29第四章白钨矿络合酸分解实验研究........................................................................................304.1实验部分........................................................................................................................304.1.1实验试剂..............................................................................................................304.1.2实验仪器及设备..................................................................................................304.1.3实验装置及操作步骤.....................