铜盐催化下含氮杂环化合物的合成分析-synthesis and analysis of nitrogen-containing heterocyclic compounds catalyzed by copper salts.docxVIP

目 录 第一章 碘化亚铜催化吡啶甲醛、二级胺、炔合成 1-氨基吲嗪 ···················· 1 1.1 文献小结 ············································································· 1 1.2 结果与讨论 ·········································································· 7 1.3 实验部分 ············································································ 15 1.4 谱学数据 ············································································ 16 1.5 参考文献 ············································································ 23 第二章 氧化亚铜纳米粒子催化合成多取代吲哚 ····································· 25 2.1 文献小结············································································· 25 2.2 结果与讨论·········································································· 31 2.3 实验部分············································································· 37 2.4 谱学数据············································································· 38 2.5 参考文献············································································· 43 第三章 CuI 纳米粒子催化的串联反应合成取代 3-亚甲基异吲哚-1-酮··········· 45 3.1 文献小结············································································· 45 3.2 结果与讨论·········································································· 50 3.3 实验部分············································································· 56 3.4 谱学数据············································································· 58 3.5 参考文献 ············································································ 64 第四章 总结 ················································································· 66 硕士期间发表的文章 ········································································ 67 附 录 ·························································································· 68 附录一：原料与试剂 ·································································· 68 附录二：仪器与设备 ·································································· 70 附录三：缩写字母英文对照表··················································