Super13Cr和13Cr不锈钢在CO2饱和的CaCl2完井液中的腐蚀行为-物理化学专业论文.docxVIP

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Super13Cr和13Cr不锈钢在CO2饱和的CaCl2完井液中的腐蚀行为-物理化学专业论文.docx

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Super13Cr和13Cr不锈钢在CO2饱和的CaCl2完井液中的腐蚀行为-物理化学专业论文

II II Abstract The stress corrosion crack (SCC) behavior of 13Cr and super13Cr in CO2-saturated CaCl2 brine was investigated by four-point bend, U-bend test, surface analysis techniques and electrochemical measurements. The critical condition and the corrosion form of SCC of super 13Cr stainless steel in CO2-containing CaCl2 brines were confirmed; and the effects of dissolved O2，temperature, brine concentration and the stress were considered in elastic zone of 13Cr and super13Cr. The study results for super 13Cr stainless steel showed that in CaCl2 brine with deoxidization, super 13Cr stainless steel mainly suffered general corrosion and stress corrosion crack. SEM morphology showed that SCC of super 13Cr stainless steel was intergranular cracking mode in the elastic zone. The critical condition of SCC of super 13Cr stainless steel in CO2-containing CaCl2 brines was confirmed when the dissolved O2 concentration was 60ppb. The decrease of dissolved O2 concentration can inhibit SCC of super 13Cr stainless steels. Potentiodynamic polarization result indicates that the corrosion rate increased with enhance of brine concentration, temperature, the stress in elastic zone. Potentiostatic polarization and potentiodynamic polarization results indicate the sensitive potential range of SCC of super 13Cr stainless steel was -400～-300mV vs. SCE. The study results for 13Cr stainless steel showed that the corrosion rate increased with enhance of brine concentration, temperature, and the stress in elastic zone. Potentiostatic polarization and potentiodynamic polarization results indicate 13Cr stainless steel mainly suffered general corrosion rather than SCC when the temperature was 125℃ and CaCl2 brine concentration was 33wt%. Keyword: 13Cr stainless steel, super 13Cr stainless steel, SCC，CaCl2, completion fluid III III 目录摘要 I HYPERLINK \l _bookmark0 Abstract II 1 文献综述 HYPERLINK \l _bookmark1 1.1 前言 (1) HYPERLINK \l _bookmark2 1.2 SCC 的形成条件和影响因数 (2) HYPERLINK \l _bookmark3