准连续网状tib2al2o32024al复合材料的制备及力学性能研究-preparation and mechanical properties of quasi - continuous mesh ti b2 al 2 o 32024 al composites.docxVIP
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准连续网状tib2al2o32024al复合材料的制备及力学性能研究-preparation and mechanical properties of quasi - continuous mesh ti b2 al 2 o 32024 al composites
哈尔滨工业大学工学硕士学位论文
哈尔滨工业大学工学硕士学位论文
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- II -
Abstract
Conventional aluminum matrix composites are usually fabricated with a homogeneous distribution of reinforcements in the matrix. This structure does not display the best ductility because the integrity of the matrix is compromised. To solve this problem, a new structural material with a network distribution was designed and prepared. 2024 Al ,TiO2 and B powders were mixed using low energy ball milling. Then network composites were in-situ fabricated by vacuum hot pressing technique. The microstructure and morphology of composites along with
the change rule of B/TiO2 were discussed using XRD、SEM and TEM. When
B/TiO2 was 2, 4/3, 0 , mechanical properties of the as-sintered and extruded composites were measured. Effects of the change rule of B/TiO2 on mechanical
properties of composites were systematically investigated..
To network structured composites, effects of the ball milling parameters on the morphology of the raw materials were discussed. 150rpm and 2h proved to be the optimum ball milling parameters. The reaction temperature was determined as
810℃ using DTA. The optimum holding time was established as 60 minutes after
studying the effects of holding time on the morphology of the reinforcements.
When B/TiO2 was 2, 4/3, 0, (TiB2+Al2O3), (TiB2+Al2O3+Al3Ti) and (Al2O3
+Al3Ti) were produced. Fine TiB2 and Al2O3 particulates both with a size of about 0.5?m,bulky Al3Ti with a size of about 25?m were observed using TEM and SEM.
Reinforcement scattered along the boundary of the 2024 Al effectively strengthened the 2024Al matrix. Also, the interpenetrating nature of the matrix contributed to the ductility of the composite.
Results of the mechanical properties at room temperature indicates that the properties of the sintered and extruded composites are enhanced with the increasing percentage of B. The mechanical properties of the composite with B/TiO2 as 2 are superior to the other two sys
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