毕业论文设计《醇相皂化与水相皂化提取米糠蜡中的高碳脂肪醇》.docVIP

PAGE 黑龙江东方学院 学 士 学 位 毕 业 论 文 醇相皂化与水相皂化提取米糠蜡中的高碳脂肪醇 学生姓名 学 号 054131117 专 业 食品科学与工程 班 级 2005—B 指导教师 学 部 食品与环境工程 黑龙江东方学院本科生毕业论文（设计） PAGE ii 醇相皂化与水相皂化提取米糠蜡中的高碳脂肪醇 摘 要 　 以米糠蜡为原料，以其中所含的高碳脂肪醇的提取为目的，提出并完成了皂化反应技术提取高碳脂肪醇的新工艺，同时完成了皂化萃取条件的优化研究。 采用以溶剂法提纯粗糠蜡得到纯度较高的精糠蜡。并优选醇相皂化和水相皂化两种方法提取获得高碳脂肪醇，选取最佳皂化方法。皂化工艺主要完成了以皂化率为考核指标的单因素范围选取的实验，在此基础上选取了以皂化时间（h）A、用碱量（倍）B、乙醇量（倍）C、乙醇浓度（C）D为因素的三因素四水平正交实验，提出了最佳工艺条件，即最佳工艺条件为：皂化时间1小时、2倍量乙醇、95%浓度乙醇、1.4倍皂化值碱量并讨论了因素及水平对皂化率的影响。 关键词：米糠蜡；高碳脂肪醇；皂化；萃取 Extract carbon alcohols from rice bran wax with the method of Alcohol saponification and aqueous saponification Abstract We use the rice bran wax as raw material, for the purpose of extraction of fatty alcohol and we completed the extraction of the saponification reaction of the new technology of carbon alcohols, at the same time , we complete the saponification Optimization of extraction conditions. We use the method of using solvent to make rice bran wax to be higher purity bran wax. And we obtain Optimization high-carbon alcohols with two ways, they are alcohol saponification and aqueous phase saponification, and we select the best method of saponification. the process of Saponificationto mainly complete a single-factor experiments which take major saponification rate as its indicators, and then we selected four factors, thet are: saponification time (h) A, alkali (times) B, ethanol volume (times) C, ethanol concentration (C) D .we make the four-factor three-level orthogonal experiment, and we abtain the optimum process conditions, the best conditions were as follows: saponification time 1 hour, 2 times the amount of ethanol, 95% concentration of ethanol, 1.4 times the volume of alkali saponification value and then we discussed the factors and the level on the impact of the rate of saponification. Key words: rice bran wax; carbon alcohols; saponification; extraction 目 录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc229927771 摘 要