蚕蛹中蚕蛹油的提取及不饱和脂肪酸的分离研究-化学工艺专业论文.docxVIP

广西大学硕士论文盏鳞中主挂娟油的lRt取及不饱和脂肪陋的分离研究 广西大学硕士论文 盏鳞中主挂娟油的lRt取及不饱和脂肪陋的分离研究 11 11 STUDY ON EXTRACTION OF THE OIL FROM SILKWORM AND SEPARATION OF POLYUNSATURATED FATTYACIDS ABSTRACT SlIkworm 011 (SCO) mainly contains polyunsaωrated fatty acids (PUFAs)， such as Iinoleic acid and a.linolenic acid ，whicb bave multiphysiological functions. There is abundant resource of silkworm in China， and it is strongly desiredωdevelop oil. 倒pecially PUFAs in SlIkworm as medicine materials，health products，etι The supercrltical C02 extraction of SCO was studled. Single factor and orthogonal experlmenωwere used ωs伽dy tbe effects of the parameters such as pressw哩， ?tempera阳re and time on the yield of SCO at C01 ?OW rate of 8kg.h.1 ? The results showed that tbe extraction pressure was the more important fac10r that affected the yield of SCO，and the optimal conditions of supercritical CO2 extraction were as follows: pressure of 2SMpa. tempera阳re of 4SC， extraction time of 2.5h，and the yield of SCO was 28.97% under extraction conditions mentioned above. The urea adduction process 01 PUFAs in SCO w划 studied. The effects of ration 01 urea to fatty acid，adduction time and temperature on purity and yield of PUFAs were discussed. The optimal adduction conditions were obtained with slngle fac10r and orthogonal experiments，as follows:ration 01ureaωEtOH of 1:3.2(W/V).ration of urea 10 fatty acid 011.5:1(W/W)，adduction temperature of S C， and adduction time of 蚕蜗中3 蚕蜗中3居蜗汹的提取及不饱和脂肪酸的分离研究 广西大学硕士论文 m m 2h ，and the yield 01 PUFAs was 70%，and the content 01 PUFAs could be raised lrom 71.0 % to 91.1 % under adduction ωnditions mentioned above ? Experiments lor separation 01 AlA衔。m SCO were performed using a刷刷US AgN03 侃阳耐。n.τbe results showed that polarity 01 extractionωIvents and comple对ng extraction temperature played m现jor role lor ωntent 01AlA from SCO at eonstant ω，neentra甜on 01AgN03 01 lmol/L.The optimalωmplexation conditlons were obtained with single lactor experimen邸， as lollows :ωnωntration 01AgN03 of2m