含硅钢纳米贝氏体组织形成分析-材料物理与化学专业论文.docxVIP

摘要针对工业用9SiCr钢，通过x射线衍射分析、金相组织观察研究了奥氏体化后的冷却 摘要 针对工业用9SiCr钢，通过x射线衍射分析、金相组织观察研究了奥氏体化后的冷却 速度与贝氏体转变等温时间等因素对贝氏体相变产物显微组织形态的影响，采用透射电 子显微镜观察分析了短时等温获得的上、下贝氏体组织的精细结构。。 实验结果表明，当奥氏体化后以20．50℃／S的冷却速度冷至380℃等温5．20 min获得非 常规上贝氏体组织，其由片条状口相亚单元组成，片条状亚单元的纵向尺寸可达几百纳 米，而宽向尺寸大约几十纳米，晶格呈现膨胀状态，相变具有非完全扩散的特征：而当 奥氏体化后以50．70℃／s冷却速度冷至200℃等温5．20 min获得非常规下贝氏体组织，透 射电镜下呈现由单一口相组成的片条状，片条的厚向尺寸处在纳米数量级，而长度处于 微米数量级，晶格呈现膨胀状态。 电镜精细结构观察发现，沿非常规下贝氏体纵向存在大体平行的位错亚结构并在纵 向前沿母相中存在层状、间断应变场衬度。该应变场为贝氏体内部的位错亚结构所萌生。 新贝氏体单元正是借助该应变场以切变机制形核，实现贝氏体沿纵向的继续长大，新形 成的贝氏体单元同时以切变机制展宽，实现贝氏体的横向生长。 对于实验用钢，短时等温获得的上、下贝氏体具有相近的显微组织结构特征，但精细 组织结构有所不同。上贝氏体由于形成温度高，生长前沿母相中形成的相变应变场容易 被原子的热振动所松弛，导致纵向生长能力减小。也正由于相变应力场的松弛，贝氏体 的横向展宽能力提高，但贝氏体各处展宽状态不同，进而在贝氏体侧边界易于形成台阶， 其为激发新的贝氏体亚单元条的形成提供条件。 关键词：9SiCr钢，冷却速度，短时等温，贝氏体纳米结构，生长机制 AbstractThe Abstract The influence of cooling rate after austenitization，isothermal time．and the cooling rate after isothermal treatment on the products of bainite transformation in 9SiCr steel has been studied by the X—Ray diffraction pattern analysis and metallographic analysis．Fine structures of upper and lower bainite formed within short isothermal time have been observed by transmission electron microscopy． The experimental results show that irregular upper bainite composed of subplates whose width is about several tens nanometers and whose length is up to several hundreds nanometers call be obtained with fast cooling rate from 20 t0 50℃／s after austenitization and isothermal time from 5 to 20 minutes．Irregular upper bainite lattice expands and its formation mechanism has the characteristic of non—wholly diffusion mechanism．Irregular lower bainite composed of口monophase can be obtained with fast cooling rate from 50 to 70℃／s after austenitization and isothermal time from 5 to 20 minutes．Under transmission electron microscopy,it is made of thin plates whose width is in the order of nano magnitude and whose length is in the order of micron magnitude． ne dislocation substructure and lamellar strain in front of the parallel interrupted