烟草中抑芽丹残留量的测定-烟草科技.PDF

　　　　　　 　　　　　　2006 7 (228 )　　　　　 1 1 1 2 　, , , 1.国家烟草质量监督检验中心, 郑州高新技术产业开发区枫杨街2 号　450001 2.中国烟草总公司职 技术培训中心,郑州市北林路7 号　450008 :抑芽丹;烟草;残留;紫外分光光度法 :采用ISO 4876-1980 规定的方法测定了239 个国产烟叶、49 个进口烟叶和12 个进口卷烟 样品中的抑芽丹残留量。结果表明:国产烟叶抑芽丹的检出率为6.69%, 最高54.00m /k , 最 低1.50m /k ,平均6.82m /k ;进口卷烟检出率为58.33%, 最高42.75m /k , 最低7.75m /k , 平均17.57m /k ;进口烟叶检出率为30.61%, 最高14.00m /k , 最低1.50m /k ,平均5.63m / k 。 + :S481 .8　:B 　:1002-0861(2006)07-0043-03 Determination of Maleic Hydrazide Residues in Tobacco ZHANG WEI (1), TANG GANG-LING (1), LIU HUI-MIN (1), and YAN HONG-YANG (2 ) 1.Zhengzhou Tobacco Research Inst tute of CNTC, Zhengzhou 450001, Ch na 2.Ch na Tobacco Tra n ng Centre for Profess onal Techn c ans, Zhengzhou 450008, Ch na Keywords:Male c hydraz de;Tobacco;Res due;UV spectrophotometry Abstract:The res dues of male c hydraz de (MH)n 239 domest c tobacco leaf , 49 mported tobacco leaf and 12 mported c garette samples were determ ned accord ng to ISO 4876-1980.The results showed that:1)the detectable rate of MH n the domest c tobacco leaves was 6.69%, the h ghest res due was 54.00mg/kg, the lowest 1.50mg/kg, and the mean value 6.82mg/kg;2 )the detectable rate of MH n the fore gn c garettes was 58.33%, the h ghest res due was 42.75mg/kg, the lowest 7.75mg/kg, the mean value 17.57mg/kg;and 3 )the detectable rate of MH n the mported tobacco leaves was 30.61%, the h ghest res due was 14.00mg/kg, the lowest 1.50mg/kg, and the mean value 5.63mg/kg . 　　,, 6-- 。 [1] [3] 2H--3- , , ,ISO 1980 , LD50 5000mg/kg[2] , 。 。, [4] , 2000 [1] 。, [3]