基质固相分散气相色谱法测定油菜籽中有机磷农药残留检测技术研究-农产品质量与食物安全专业论文.docxVIP

AbstractThe Abstract The tJ∞of p蒯des provides unquestionable benefits in increasing agricultural production． However,the problm of pesticide residues has potential risk to coflsuuler$．China is big rape$∞d produced country and rapeseed is the main$ourcz ofedible oil and feed protein．Take some research the technique of pesticide residues test will have significance the improving of矾and on product quality and the healthy ofpeople．The oil content ofrapeseed a【ceed 40％．high fat content will do some harm to the column and signal compress．How to separate and purify pesticide residues from lmpcsoed is the key of the establishment of test technique．This article focus extracting end cleaning up 14 organophagphnrm pesticide residues from ap∞∞d’and optimizing the condition ofgag chromatogram．A test method of 14 orgenophesphnms pesfcide residues in rapesoed wag established． Themainresultsofthispaperagfollowed： 1．In this reses∞ch,matrix soiid-phase dispersion method was used to cotllact and purify pesticides from rapeseed．for the high on content,We optimized the agorbent,elute and the materials for Momldary cleaning up,established preparation method which used 29 florisil absorbent,10mL acetone eluto and the rate ofsample and filling wagl：4．ODS-Cnend actived cAlrboll w哪taken secondarycleaning-upmaterialsbysoliddispersion cleaningupmeiho 2．A study the type ofcolumn and the condition ofgas chromatogram Wag carried out in this paper,GC detection method oforganophosphorag pesticide residues Wag established．Adding different level standard materials to blank for the test ofrecovery,the nⅫits showed that the recovery range was 79．9％～l 13．3％with relatiVe standard deviation lower than lO％which indicated the method satisfied the demand pesticide residue analysis．Compared with the nation method．the recoveries increased for 7．3-39．9％． 3．140 Samples WM collected from the main舟pcseed product∞8 in ommtty for 14 伪学mol，h∞ph‘肺u8 insecticides detected using the established method．，5 orgenophosphor