棉籽综合利用加工工艺的研究-农业生物环境与能源工程专业毕业论文.docxVIP

棉籽综合利用加工工艺的研究-农业生物环境与能源工程专业毕业论文.docx

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II II 棉籽综合利用加工工艺的研究业化生产,有利于降低生产成本。 棉籽综合利用加工工艺的研究 2. 双液相萃取棉籽能够提油脱酚,棉油可以用来生产生物柴油,棉酚,棉籽糖能够被提取,棉 粕能提蛋白或做饲料,从而增大棉籽的使用价值。 关键词:生物柴油;棉籽毛油;双液相萃取; 棉酚;棉籽糖 PAGE PAGE IV 棉籽综合利用加工工艺的研究 棉籽综合利用加工工艺的研究 Abstract Objective: For hulled cottonseed as raw material, using two immiscible solvents to double liquid extraction, for extraction of oil, and removal gossypol, to extract the oil for biodiesel production by chemical method , and research the process of raffinose and gossypol extraction ,sametime study cottonseed crude oil by simple alkali refining,then find the transesterification reaction conditions on the yield of fatty acid methyl ester to obtain better conditions. Study the utilization of the cottonseed processing, in order to achieve maximum use of the value of cottonseed. Method: Experiment using two-phase extraction method, the phenol removal cottonseed oil extraction, oil extracted to producte biodiesel, the content of gossypol using UV spectrophotometer to test, using water dilution to purify gossypol. Raffinose extraction by the ethanol contain water from the cottonseed , methanol phase after removal the extraction of gossypol can obtain the raffinose. Cottonseed oil through a easy alkali alkali refining, then centrifugal separation, removal of soap foot to obtain cottonseed oil can be used to producting biodiesel, through single factor experiments and orthogonal experiments, can get the level of reaction conditions. HPLC and TLC to be use analysis of biodiesel components. Results: Two-liquid extraction of cottonseed, methanol phase content the gossypol to 0.544%, after the removal of phenol removal oil and the free gossypol in cottonseed meal contain the free gossypol is 0.02% , bellowed the national standard of 0.04%, can be use in protein feed area development and utilization. Gossypol content in cottonseed crude oil was 0.108%,after alkali refining content reduced to 0.032%, quality get greatly improved. Water miscible ethanol can be used to extraction raffinose in

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