低熔点玻璃粉包覆FeSiAl合金的结构和电磁性能.pdf

第33 卷 第6 期 Vol. 33 No. 6 2019 年6 月 CHINESE JOURNAL OF MATERIALS RESEARCH Jun. 2019 低熔点玻璃粉包覆FeSiAl 合金的结构 和电磁性能 张达理 刘育建 方俊 (华东理工大学材料科学与工程学院 上海 200237) 摘要 将低熔点玻璃粉D250 绝缘包覆剂与扁平化的FeSiAl 合金粉末机械混合，进行热处理使D250 熔融流动 而包覆在片状FeSiAl 粉末表面。借助XRD ，SEM ，XRF 和EDS 等手段研究了包覆后粉末的物相组成、表面形 貌和元素组成；用矢量网络分析仪测试了材料在1~ 18 GHz 频率范围内的电磁参数和反射损耗。结果表明，熔 融包覆后的粉末形成均匀致密的包覆层，其复介电常数的实部降低到8 左右。热处理温度为700℃时材料的 最大反射损耗降至-40.10dB ，有效频宽达到3.76 GHz 。 关键词 金属材料，FeSiAl 合金，熔融包覆，吸波性能 中图分类号 TM25 文章编号 1005-3093(2019)06-0475-06 Structure and Electromagnetic Properties of Glass D250 Coated FeSiAl Alloy Flakes ZHANG Dali, LIU Yujian, FANG Jun (School of Materials Science and Engineering, East China University of Science and Technology, Shanghai 200237, China) Correspondent: LIU Yujian, Tel: (021 E-mail: yjliu@ecust.edu.cn Manuscript received 2018-12-06, in revised form 2019-03-02 ABSTRACT FeSiAl alloy flakes were coated with glass powder D250 of low melting point via a two- step process, i.e. FeSiAl alloy flakes and glass powders D250 were firstly blended by ball milling to pre- pare D250 powders covered FeSiAl alloy flakes and then which was heat treated at proper elevated tem- perature. The phase composition, surface topography and composition of the coated flakes were charac- terized by using XRD, SEM, XRF and EDS . The electromagnetic parameter and reflection loss were also assessed in the frequency range of 1~18 GHz by using v