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第三章 填充纳米复合材料 Top view and cross-sectional view FESEM images of (A, A’) TiO2 prepared by an anodization in HF–H3PO4–EG–H2O electrolyte and NiO–TiO2 nanocomposites through a (B, B’) one-cycle or (C, C’) multi-cycle electrodeposition–oxidation synthesis. (4) The dispersion of SWCNTs treated by dispersing agents in glass fiber reinforced polymer composites It is an obstacle issue for carbon nanotubes (CNTs) particularly for single-wall carbon nanotubes (SWCNTs) with nano-level dispersion in fiber reinforced polymer matrix composites. In this paper, the dispersing agents such as Volan and BYK-9076 were employed to treat SWCNTs to improve their dispersion in the glass fiber/epoxy (GF/EP) composites. The dispersing results of SWCNTs in composites were observed by scanning electron microscopy (SEM). Then the glass transition temperature (Tg) of these kinds of composites with treated and untreated SWCNTs were obtained by dynamic mechanical thermal analysis (DMTA). Moreover, the flexural tests were performed on these composites. Based on the experiment results, the dispersion of SWCNTs was improved and the flexural property of SWCNTs/GF/EP composite was enhanced too. 第三章 填充纳米复合材料 The SEM micrographs of J2 composite with untreated SWCNTs at different magnification The SEM micrographs of J4 composite with SWCNTs treated by Volan and BYK-9076 第三章 填充纳米复合材料 (5) Nano-porous SiO/carbon composite anode for lithium-ion batteries Carbon-coating of sub-μm SiO particles (dmax = 0.36 μm,) by a fluidized-bed chemical-vapor-deposition process has produced unique nano-porous SiO/C secondary particles within which the SiO primary particles are ‘‘glued’’ together by carbon to form a network that possesses randomly distributed pores with sizes in the nano-meter range and a bulk porosity of 30%. Upon lithiation/ delithiation cycling in an organic Li-ion electrolyte, the electrode made of the SiO/C particles exhibited reduced polarization, smaller irreversible electrod
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