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‘Special Topics for NMR Spectroscopy’Course Syllabus
Course CodeCourse Category:专业选修课程 Major elective
Majors:Chemistry, Chemical Engineering
Semester:Fall
Total Hours:36 Hours Credit:2 学分
Lecture Hours:36 Hours Lab Hours:0 学时 Practice Hours:0 学时
Textbooks:R. M. Silverstein et al., Spectrometric Identification of Organic Compounds, 8th Ed., Wiley, 2014.
References:
R. M. Silverstein et al., Spectrometric Identification of Organic Compounds, 8th Ed., Wiley, 2014.
M. H. Levitt, Spin Dynamics: Basics of Nuclear Magnetic Resonance, Wiley, 2005.
J. Keeler, Understanding NMR, Wiley, 2005.
S. Braun et al., 150 and More Basic NMR Experiments, 2nd Ed., Wiley, 1999.
Teaching Aim:
This course will focus on the basic theory of how NMR spectroscopy works, fundamentals of Fourier transform spectroscopy, maximizing the available spectral information, data quality and reliability through optimization of data collection and processing parameters. It intended for advanced undergraduate and beginning graduate students who expect to collect and process their own data. There will be discussions and examples of how to recognize bad/unreliable data, the best way to present spectroscopic data, when an experiment should be repeated, and difference between acceptable and unethical data manipulation. Concepts will be illustrated with a generous number of figures from real spectral data of small molecules and polymers. Underlying themes throughout the course will also include the scientific method, ethics in science and spectroscopy, and environmental issues. These will be discussed by comparing and drawing parallels between spectroscopic data and digital photography. Generous use of striking digital images from international world heritage sites will be used for this purpose.
Chapter One Fundamental NMR
课时:1周,共2课时
Contents
What causes nuclear spin
Interaction of nuclear spin with a magnetic field
Spin polarization, magnetic moment, Boltzmann distribut
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