草豆蔻正丁醇部位化学成分.pdfVIP

ChemicalConstituentsin ．butanolExtractfr0m the seeds。fAlpi LIYuan—Yuan1，2，3CHOU Gui—Xin1，2 WANG Zheng—Tao1，2 ， ， iTheMOEKeyLaboratoryforStandardizationofChineseMedicines． InstituteofChineseMateriaMedicn．Shahgh口iUniversi}y TraditionalChineseM edicine，Shanghai201203； ShanghaiRDCenterforStandardizationofChineseMedicines,Shanghai201203； ZhejiangMedicalCollege，Hangzhou310053，China A【BSTRACT]AIM：T0studythechemicalconstituentsinn—butanolextractfromseedsofAlpiniakatsumadaiHayata．． M ETH0DS：Variouschromatographicmethodswereapplied toisolatepurecompoundsand theirstructureswereelu— cidatedbyspectroscopicmethods．RESUI S：Tencompoundswereisolatedandtheirsturctureswerejdentifiedas quercetin3-O一(2，6-di—O—rhamnopyranosylgalactopyranoside)(1)，isorhamnetin 3-O一(2，6-di—O—rhamnopyranosylga— lactopyranoside)(2)，pinocembrin一3，7-di-p-D—glucoside(3)，quercetin3-O—robinobioside(4)，catechin(5)，adenosine (6)，uracil(7)，nicotinicacid(8)，hypoxanthine(9)andadenine(1O)．C0NCLUSIoN：Allcompoundsarefirstlyiso一 1atedfrom thisplantandcompounds1-4，6—10wereisolatedfrom thegenusAlpiniaRoxb．forthefirsttime． K【EYWoRDS】A／piniakatsumadai；Flavonoids；Nitrogenouscompounds C【LCNumber】R284．1 D【ocumentcode】A A【rticleID】1672—3651(2009)06—0417—04 doi：1013724／SR J．1009．2009．00417 A inia katsumadaiHayata．(Zingiberaceae)grows cetm 3-O—robinobioside (4)，catechin (5)，adenosine (6)， wildmainlyinHainan，GuangxiandGuangdongprovinces uracil(7)，nicotinicacid(8)，hypoxathine(9)，adenine(10)． inSouthern China；itsseed isavery commontraditional Allcompoundswerefirstlyisolatedfrom thisplantandthe Chinesemedicine．Itisrecorded intheChinesePharma— compounds1-4，6-10wereisolatedrfom thegenusAIpinia copoe