进出口动物源食品中多种米尔贝霉素残留量的测定英文意见稿.docVIP

Foreword This standard was drafted by GB/T 1.1-2009. Annex A, B amd C of this standard is an informative annex. This standard was proposed by and is under the charge of the Certification and Accrediation Administration of People’s Republic of China. The standard was drafted by Shenzhen Entry-Exit Inspection and Quarantine Bureau of the People’s Republic of China, Shenzhen Academy of Inspection and Quarantine. The main drafters of this standard are Kang Haining, Yue Zhenfeng, Li Yong, Xie Liqi，Ouyang Shan, Lin Li, Hou Lexi, Shen Jincan. This standard is a professional standard for entry-exit inspection and quarantine promulgated for the first time. Please note that some of the content of this article may be involved in the patent, the publisher of this document does not assume the responsibility to identify these patents. Determination of milbemycins residues in foodstuffs of animal origin for import and export ---- LC-MS/MS method Scope This standard specifies the methods of determination by liquid chromatography - tandem mass spectrometry of moxidectin, milbemycin A3, milbemycin A4, milbemycin D, nemadectin in foodstuffs of animal origin. This standard is applicable to the determination and conformation of moxidectin, milbemycin A3, milbemycin A4, milbemycin D, nemadectin in chicken, pork, beef, chicken liver, pig liver, beef liver, chicken liver, chicken kidney, egg, milk and fish. Quoted normative documents The following documents for the application of this document is essential. For dated references, only the dated version applies to this document. For undated references, the latest version (including all amendments) applies to this document. GB/T 6682 Water for analytical laboratory use --- Specification and test methods Abstract The residues of milbemycins in the test sample (besides milk) were extracted with tert butyl methyl ether, the extraction was evaporated under nitrogen blow and then redissolved, purified and concentrated on a silica SPE column, the