长春七二氧化碳超临界萃取物的化学成分的研究.pdfVIP

长春七二氧化碳超临界萃取物的化学成分研究 1 1 1 1 石娟 靳菊情 马婧 边敏 西安交通大学药学院 陕西 西安 710061 摘要 目的 研究长春七[Libanotis buchtorimensis (Fisch) DC.]中挥发油的化学成分 方法 采 用二氧化碳超临界萃取法提取长春七挥发油成分 运用 GC-MS进行分离测定 结合计算机检索技术 对分离的化合物进行结构鉴定 应用色谱峰面积归一化法测定各成分的相对百分含量 结果 二氧 化碳超临界萃取物提取率为 4.19% 分离出 31 个化合物 鉴定出 11 个化学成分 结论 超临界萃 取法具有耗时少 准确 效率高和提取完全等优点 关键词 长春七 化学成分 超临界萃取 GC-MS Studies on the chemical constituents of the volatile oil from the roots of Libanotis buchtorimensis by supercritical fluid extraction 1 1 1 1 SHI Juan JIN Juqing MA Jing BIAN Min (1.Xian Jiaotong University, College of Pharmacy Xian 710061 China ) ABSTRACT OBJECTIVE To study the chemical constituents of the volatile oil from the roots of Libanotis buchtorimensis (Fisch) DC.. METHODS The essential oil was obtained by supercritical fluid extraction SFE The chemical compositions were separated and identified by GC-MS.The relative contents in the essential oil were determined by area nomalization .RESULTS The extraction efficiency of supercritical fluid extraction wes 4.19 %, and 31 chemical constituents were separated and 11 chemical constituents were identified. CONCLUSION The SFE method demonstrated many advantages,such as short extraction time, and accurate with high extraction efficiency,etc. KEY WORDS Libanotis buchtorimensis; chemical constituents; SFE; GC MS 长春七[Libanotis buchtormensis (Fisch) DC.]是伞形科岩风属植物 产于陕西秦岭山 脉 在甘肃 四川等省也有分布 长春七是陕西特有的中草药 药用其根 有发散风 湿