试样对纯净钢元素分析影响浅析.pdfVIP

2007年第 3期 宝 　钢 　技 　术 49 试样对纯净钢元素分析影响浅析 胡会军 ,柳 　凯 (宝钢分公司 　炼钢厂 ,上海 　20094 1) 　　摘要 :随着钢质纯净度的不断提高 ,需要分析的钢中气体元素含量以及部分低碳钢的碳含量越来越低 ,分 析精度要求越来越高 。对大生产中分析气体氢使用的真空玻璃吸管棒样以及分析氧和碳使用的扁平样和双 厚度样进行了分析 ,认为上述取样器用于氢 、氧和碳分析时波动较大 ,精度不能满足要求 ,而对氮的分析没有 影响 ; 同时认为在线定氢仪和 TO S取样器取出的试样成分稳定 ,具有很好的代表性 ;研究表明不同的加工方 式对试样的分析精度也会产生较大的影响 。 　　关键词 :纯净钢 ;取样器 ;分析精度 中图分类号 : TG115. 3　文献标识码 : B 　文章编号 : 1008 - 07 16 (2007) 04 - 0049 - 04 Effect of Sam p les on Ana ly sis of E lem en ts in C lean Steels H u H u iju n , L iu Ka i ( Steelm ak ing P lan t, Bao steel Branch, Shangha i 20094 1, Ch ina ) 　　A b stract:A s steels becom e p urer and p urer, som e gas elem ents in steels are needed to be analyzed, and carbon conten t in som e low carbon steels becom e lower and lower, wh ich lead s to h igher requ irem en ts for analytical accu ra cy. The accuracy of the vacuum glass tube samp ler u sed to analyze gas hydrogen in m a ss p roduction was discu ssed, together w ith that of the p addle and dualth ickne ss samp lers for carbon and oxygen analysis. The re su lts show that these samp le s are not stab le, and their accu racy cannot m eet the dem and of the p roduction, but the se samp lers do not affect the analysis of ga s n itrogen. It wa s believed that the on line hydrogen tester and TO S samp ler turned out to be better for samp les taken by the se samp lers did not fluctuate in elem en t con ten ts, and were very rep resen tative. The re search indicates that the effect of different p roce ssing m ethod s on analytical accuracy of samp les is great. Keyword s: clean steel; samp ler; analytical acc