PVA-assisted synthesis and characterization of core–shell Bi nanobelts》.pdf

PVA-assisted synthesis and characterization of core–shell Bi nanobelts》.pdf

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PVA-assisted synthesis and characterization of core–shell Bi nanobelts》.pdf

Materials Letters 161 (2015) 144–148 Contents lists available at ScienceDirect Materials Letters journal homepage: /locate/matlet PVA-assisted synthesis and characterization of core–shell Bi nanobelts Xing Yu a, Yves Fautrelle b, Zhongming Ren a, Xi Li a,b,n a Department of Materials Engineering, State Key Laboratory of Advanced Special Steels, Shanghai University, 200072 Shanghai, PR China b SIMAP-EPM-Madylam/CNRS, ENSHMG, BP 95, 38402 St. Martin d ’Heres Cedex, France a r t i c l e i n f o a b s t r a c t Article history: A facile large-scale hydrothermal process was proposed to synthesize core–shell nanobelts with single- Received 11 June 2015 crystalline Bi nanobelts as cores that may be resulted from the pseudolayered structure and poly(vinyl Received in revised form alcohol) (PVA) as shells in which PVA chains reduced sodium bismuthate in mixed solution. The results 28 July 2015 have demonstrated that the formation of such Bi nanobelts is controlled by seed-mediated growth in an Accepted 16 August 2015 Ostwald ripening process, in which Bi nanostructures evolved through repetitive crystalline–amorphous Available online 18 August 2015 transformations. In addition, STEM–EDS and HRTEM have confirmed that the shells of Bi nanobelts are Keywords: indeed as same as the transparent amorphous Bi nanobelts composed of amorphous Bi and PVA. Single-crystalline Bi nanobelts

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