Pyrene-appended imidazolium probes as 3,5-dinitrosalicylic acid sensors in 10% aqueous media》.pdf
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Pyrene-appended imidazolium probes as 3,5-dinitrosalicylic acid sensors in 10% aqueous media》.pdf
Dyes and Pigments 122 (2015) 351e358
Contents lists available at ScienceDirect
Dyes and Pigments
journal homepage: /locate/dyepig
Pyrene-appended imidazolium probes as 3,5-dinitrosalicylic acid
sensors in 10% aqueous media
*
Ashwani Kumar, Anup Pandith, Hong-Seok Kim
Department of Applied Chemistry, School of Applied Chemical Engineering, Kyungpook National University, Daegu 702-701, Republic of Korea
a r t i c l e i n f o a b s t r a c t
Article history: Pyrene-appended imidazolium salts (1 and 2) were synthesized for sensing of salicylic acids and they
Received 14 June 2015 selectively and sensitively detected 3,5-dinitrosalicylic acid (3,5-DNSA) in pH 7.4 PBSeEtOH (1:9) solu-
Received in revised form 1
tion. The interaction of 3,5-DNSA with 1 and 2 was examined by UVevisible, fluorescence, and H NMR
6 July 2015
spectroscopy and was supported by DFT calculations. The binding of 3,5-DNSA to probe 2 leads to
Accepted 8 July 2015
complete quenching of its green excimer emission because of loss of pep interactions between the
Available online 17 July 2015
pyrene rings and energy transfer from electron-rich pyrene to electron-deficient 3,5-DNSA. Binding of
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