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NREL Update—CAFI 2 Teleconference Rick Elander National Renewable Energy LaboratoryNational Bioenergy CenterGolden, CO February 18, 2004 Outline Dilute Acid Pretreated Corn Stover Data Dilute Acid Pretreated Hybrid Poplar Data (Bench Scale-Steam Gun) Description of Dilute Acid Pretreated Hybrid Poplar (Pilot Scale-Sunds Reactor) Data not yet available Dilute Acid Pretreated Corn Stover Feedstock: 2nd pass corn stover from Kramer farm (Wray, CO) Collected using high rake setting to avoid soil pick-up Milled to pass 0.25 inch screen (Mitts and Merril knife mill) Pretreated in Sunds vertical reactor, with and without hot washing Pilot Scale Sunds Vertical Reactor Dilute Acid Pretreated Corn Stover Pretreatment Conditions: Typical “mid severity” condition in the Sunds vertical pretreatment reactor (190 C, ~ 1.5 minute residence time in “flowthrough mode”, 0.045 g sulfuric acid/g dry feedstock, 30% insoluble solids) ? “Low severity” condition in the Sunds vertical pretreatment reactor (180 C, ~ 1.5 minute residence time in “flowthrough mode”, 0.03 g sulfuric acid/g dry feedstock, 25% insoluble solids) ? “Low severity” condition in the Sunds vertical pretreatment reactor (180 C, ~ 1.5 minute residence time in “flowthrough mode”, 0.03 g sulfuric acid/g dry feedstock, 25% insoluble solids) and hot washed in Pneumapress pressure belt filter with hot water. Dilute Acid Pretreated Corn Stover—Pretreated Solids Composition and Component Solubilization Dilute Acid Pretreated Hybrid Poplar (Bench Scale-Steam Gun) Feedstock: USDA-supplied hybrid poplar (Alexandria, MN) Debarked, chipped, and milled to pass 0.25 inch screen (Mitts and Merril knife mill) Pre-impregnated with H2SO4 and pretreated in 4 L NREL steam gun Composition of Pretreated Solids from Dilute Acid Pretreated Hybrid Poplar (Bench Scale-Steam Gun) Composition of Pretreated Liquids from Dilute Acid Pretreated Hybrid Poplar (Bench Scale-Steam Gun) Glucose and Xylose Component Balance from
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