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Determination on pain Tincture Piper longum content of piperine
PAGE \* MERGEFORMAT 9
Determination on pain Tincture Piper longum content of piperine
[Abstract] Objective To establish a Piper longum pain tincture method for the determination of piperine. Methods HPLC, C18 column, tetrahydrofuran - methanol - water (V: V: V = 30:30:50) as mobile phase The flow rate was 1.0 mL / min, column temperature was at room temperature, detection wavelength was 343 nm, injection 10 μL, other than the standard method content. Results of piperine in the 8.3 ~ 41.5 mg / L reference substance within the peak area and concentration was good linear relationship, the regression equation: A = 3 413 186ρ-
7 467.7, r = 0.999 8, the average recovery was 99.7%, RSD = 1.8% (n = 6). Conclusion The method is simple, reproducible, and the blank without interference, which can effectively control the pain Piper longum quality tincture preparations .
[Keywords:] Piper longum pain tincture, piperine, high performance liquid chromatography
Abstract: Objective To establish the method of content determination of Piperine in Biba Zhitong Tincture. Methods HPLC was adopted in determining the content of piperine in Biba Zhitong Tincture. C18 chromatographic column was used with the column temperature being the room temperature. The mobile phase was tetrahydrofuran-methanol-water (V: V: V = 30:30:50) with the velocity of 1.0 mL / min. The detection wavelength was 343nm, and the sampling volume was 10 μL. External standard method was chosen for content calculation. Results The inner peak area of #8203;#8203;piperine (8.3 ~ 41.5 mg / L) showed fine linear relation with mass concentration of control group. Its regression equation was A = 3 413 186ρ-7 467.7, r = 0.999 8, with the average recovery ration being 99.7%, and RSD = 1.8% (n = 6). Conclusion The method is simple, convenient, good reproducibility and non-interference, and can effectively control the quality of the preparation.
Keywords:: Biba Zhitong Tincture, Piperine, HPLC
Piper longum
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