HPLC Determination of rhinitis Ling pills magnolin content.docVIP

 PAGE \* MERGEFORMAT 9 HPLC Determination of rhinitis Ling pills magnolin content [Abstract] Objective To establish a reversed-phase high performance liquid chromatography (HPLC) Determination of rhinitis Ling pills magnolin concentration method. Methods using high performance liquid chromatography. Column: Diamonsil C18 (4.6mm * 200mm); mobile phase: acetonitrile - tetrahydrofuran - water (44:1:55); detection wavelength: 278nm; flow rate: 1.0ml/min; column temperature: 30 ℃ . Results magnolin in the range of 0.3156 ~ 1.8936μ g a good linear relationship, r = 0.9999, average recovery was 96.6%, RSD 1.8%. Conclusion The method is simple, accurate, high sensitivity, good stability, can effectively control the quality of rhinitis Ling Wan. [Keywords:] high-performance liquid chromatography; rhinitis Ling Wan; magnolin Determination of magnolin in biyanling pill by HPL [Abstract] Objective To establish a method for determination of the content of magnolin in Biyanling pill by HPLC.Methods The HPLC method was used, The analytical column was Diamonsil C18 column (4.6mm * 200mm), The mobile phase consisted of acetonitrile-tetrahydrofuran -water (44:1:55), the detector wavelength was 278nm, the flow rate was 1.0ml/min, and the column temperature was 30 ℃ . Results The calibration curve was linear (r = 0.9999) in the range of 0.3156 ~ 1.8936μ g for magnolin.The average recovery of the method was 96.6% with RSD 1.8%. Conclusion The method is simple, accurate, sensitive and stable, and can be used for the quality control of Biyanling pill. [Keywords:] HPLC; biyanling pill; magnolin Rhinitis Ling Wan for the Ministry of Health standards for traditional Chinese medicine set prescription drug formulations 10th book containing relevant species, with Qufeng heat, swelling Tongqiao role, mainly by Xanthium, Magnolia, Angelica and other drug composition Bawei for nasosinusitis, nasal congestion, nasal flow of turbid tears and other acute and chronic rhinitis [1]. The origi