Qi Capsule Quality Standards.docVIP

 PAGE \* MERGEFORMAT 5 Qi Capsule Quality Standards [Abstract] Objective: To establish a stilbene capsule quality standards. Methods: HPLC determination of ginsenoside Rg1 and the preparation of the content of Re. Results: Ginsenoside Rg1 in the context of 2.6μ g ~ 8.84μ g showed good linear relationship, R = 0.9997; ginsenoside Re in the context of 2.120μ g ~ 7.208μ g showed good linear relationship, R = 0.9990. Conclusion: The method is simple and feasible, sensitive and accurate, specific and reproducible. [Keywords:] Qi Capsule; high-performance liquid chromatography; Ginsenoside Rg1; Ginsenoside Re Qi Capsule is Astragalus, ginseng, Sophora medicinal herbs such as the composition of compound preparation, with Qi righting, enhance immune function. For primary liver cancer, lung cancer, colorectal cancer, all kinds of causes leukopenia. In order to process this preparation to control the production and finished products, its main components in ginseng ginsenoside Rg1 and Re were determination, reported as follows. An instrument and reagent High-performance liquid chromatography: the United States Waters600 pump, 486 UV detector, manual injector 7725, Ginsenoside Rg1 and Re by the Chinese pharmaceutical and biological products to offer pure acetonitrile for chromatography, water re-distilled water; Qi Capsule for the White Mountain pharmaceutical products. 2 Methods and Results 2.1 Chromatographic conditions using octadecyl silane bonded silica gel as a filler; with acetonitrile: water: trifluoroacetic acid (1M) (21:79:1) as the mobile machine, detection wavelength of 203nm. 2.2 Preparation of reference substance solution precision Weigh Ginsenoside Rg1 and Re reference substance appropriate, Chi brown Liang Ping, add methanol produced per 1ml of solution containing 0.52mg and 0.424mg, that was (10 ℃ below saved). 2.3 Preparation of solution for the test materials to take this product 2.0g preparation, precision, said fixed with 100ml distil