The forefront of the quality standard for XK.docVIP

 PAGE \* MERGEFORMAT 14 The forefront of the quality standard for XK Author: small cotton farmers, LIANG Yong-ping, WEI Min Method [Abstract] Objective To study the forefront of XK and the establishment of quality standards. Methods The thin-layer chromatography (TLC) of the tablets in the cork, red peony, Chinese angelica, Chuanxiong qualitative identification; using RP-HPLC (RP-HPLC) determination of berberine hydrochloride tablets. TLC has the exclusive results. HPLC accurate and reliable. Berberine 0.104 ~ 1.040 μ g showed good linear relationship within the framework of (r = 5), the average recovery was 99.71%, RSD = 1.95% (n = 6). Conclusion The method is sensitive, accurate and can effectively control the forefront of shu quality. [Keywords:] the forefront of shu; berberine; quality control; thin-layer chromatography; high-performance liquid chromatography Abstract: ObjectiveTo establish and study the quality standard for Qianlieshu tablet.MethodsCortex Phellodendri Chinese, Radix paeoniae rubra, Radix Angelicae Sinensis, Rhizoma Chuanxiong were identified by TLC, and herbaceous peony content in capsule was determined by RP-HPLC. ResultsTLC method was specific, HPLC method was accurate and reliable.The Berberine Hydrochloride of the Cortex Phellodendri Chinese showed a good linear relationship in the range of 0.104 ~ 1.040μ g (r = 5) and average recovery was 99.71%, RSD = 1.95% (n = 6). ConclusionThis method is sensitive, accurate and can be used to control the quality of the Qianlieshu tablet. Keywords:: Qianlieshu tablets; Berberine Hydrochloride of Cortex Phellodendri Chinese; Quality control; TLC; HPLC Qianlieshule films are heat Lishi, Huayu Sanjie efficacy, mainly for chronic prostatitis, prostatic hyperplasia, urinary frequency, urinary urgency, urine pouring Lek, perineal bulge and so on. Their prescriptions from the cork, red peony, Chinese angelica, Chuanxiong composed of 13 Chinese herbal medicines for the study of new drugs in Guangxi