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The more the quality of the liver capsule Standards
PAGE \* MERGEFORMAT 18
The more the quality of the liver capsule Standards
【Abstract】 Objective To establish more control over the liver capsule quality standards. Methods of liver capsule more major components of Salvia, gardenia, Treats, Astragalus, Schisandra carried out TLC; using high performance liquid chromatography determination of the content of baicalin. The results can be thin-layer chromatography in the preparation of red sage root, gardenia, Treats, Astragalus, Schisandra to make an accurate identification; baicalin linear range of 0.12 ~ 0.58 μg, r = 0.999 7, the average rate of sample collection rate of 99.06, RSD is 1.40 (n = 5). CONCLUSION This method is sensitive, simple, reproducible, and can be used for quality standards.
Keywords: Liver capsule baicalin more high-performance liquid chromatography TLC
Abstract: ObjectiveTo establish the quality standard for Ganyu Capsule.MethodsRadix Salviae Miltiorrhiae, Fructus Gardeniae, Cortex Phellodendri, Radix Astragali and Fructus Schisandrae were identified by TLC. Baicalin was determined by HPLC. ResultsTLC spots developed were fairly clear, and the blank test showed no interference. Baicalin showed a good linear relationship in the concentration range of 0.116 8 ~ 0.584 0 μg, and the average recovery was up to 99.06%, RSD was 1.4%. ConclusionThe method is accurate, reproducible and simple. It can be used as the quality control of this preparation.
Keywords:: Ganyu Capsule; Baicalin; TLC; HPLC
The more the liver capsule by the skullcap, red sage root, gardenia, Treats, Astragalus, Schisandra and other traditional Chinese medicine, has a heat-clearing and detoxifying, Yiqihuoxue effect. Indications Qi and Yin Deficiency hepatitis. To control the inherent quality of the product, the present study, TLC, HPLC and other methods of quality standard for them.
An instrument and reagent
Waters600E 2487 High Performance Liquid Chromatography (United St
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